If you have stable product you should use SiO2 - 40 and Celite on the top of silica 'flash pomp system'. By using this system, you will get rid of every form of a palladium species and triphenylphosphine oxide. Good luck :)
If you have stable product you should use SiO2 - 40 and Celite on the top of silica 'flash pomp system'. By using this system, you will get rid of every form of a palladium species and triphenylphosphine oxide. Good luck :)
Dear Lee,
You just need to wash it with cold MeOH and filtered-off.
Regards,
Dear Lee,
You just need to wash it with cold MeOH and filtered-off.
Regards,
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Enrico Perspicace this procedure remove the oxidized phosphine?
Enrico Perspicace this procedure remove the oxidized phosphine?
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Dear Lee,
You just need to wash it with cold MeOH and filtered-off.
Regards,
Dear Lee,
You just need to wash it with cold MeOH and filtered-off.
Regards,
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Thank you so much!
Thank you so much!
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If you have stable product you should use SiO2 - 40 and Celite on the top of silica 'flash pomp system'. By using this system, you will get rid of every form of a palladium species and triphenylphosphine oxide. Good luck :)
If you have stable product you should use SiO2 - 40 and Celite on the top of silica 'flash pomp system'. By using this system, you will get rid of every form of a palladium species and triphenylphosphine oxide. Good luck :)
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Dear Lee, If you have stable product You should use SiO2 40.
Dear Lee, If you have stable product You should use SiO2 40.
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Mariusz Majchrzak using wich solvent?
Mariusz Majchrzak using wich solvent?
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