9H-Fluoren-9-amine, hydrochloride (1:1)

WHITE TO BEIGE CRYSTALLINE POWDER

First step, 9-fluorenone oxime (400 mg) and concentrated HCl (0.86 ml) in EtOH (50 ml) was subjected to hydrogenation at atmospheric pressure in the presence of 10percent Pd/C (33 mg). The reaction solution was filtered and the filtrate was concentrated. The residue was suspended in EtOAc, and the suspension was filtered to yield fluorenamine hydrochloride (240 mg) as a white solid.weigh precisely 9-fluorenone oxime (400 mg) and add 10percent Pd / C (33 mg) and concentrated hydrochloric acid (0.86 mL), dissolved in EtOH (50 mL), hydrogenated under atmospheric pressure , Filter the reaction solution, remove Pd / C, evaporate the filtrate, add ethyl acetate, mix well, Dissolve, filter to give pale yellow solid 9-fluorene hydrochloride (240 mg)

Molecular Weight:217.69
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:1
Exact Mass:217.0658271
Monoisotopic Mass:217.0658271
Topological Polar Surface Area:26
Heavy Atom Count:15
Complexity:191
Covalently-Bonded Unit Count:2
Compound Is Canonicalized:Yes