N-Boc-(S)-2-amino-3-benzyloxy-1-propanol
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N-Boc-(S)-2-amino-3-benzyloxy-1-propanol
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CAS No:
79069-15-1
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Formula:
C15H23NO4
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Chemical Name:
N-Boc-(S)-2-amino-3-benzyloxy-1-propanol
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Synonyms:
BOC-O-BENZYL-D-SERINOL;BOC-O-BENZYL-L-SERINOL;BOC-D-SER(BZL)-OL;BOC-D-SERINOL(BZL);BOC-(S)-2-AMINO-3-PHENYLMETHOXY-1-PROPANOL;BOC-(R)-2-AMINO-3-PHENYLMETHOXY-1-PROPANOL;BOC-SERINOL(BZL);BOC-SER(BZL)-OL
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CAS No:
N-Boc-(S)-2-amino-3-benzyloxy-1-propanol Basic Attributes
281.35
281.162720
DTXSID80560157
2924299090
Characteristics
67.8
1.7
1.1±0.1 g/cm3
66-69 °C(lit.)
221.8±27.3 °C
1.516
Store at 0-5°C
-14 º (c=1 in chloroform)
N-Boc-(S)-2-amino-3-benzyloxy-1-propanol Use and Manufacturing
To a stirred solution of 28 (9.28 g, 31.7 mmol) and N-methyl morpholine (3.7 mL, 33.7 mmol) in DME (70 mL) was added isobutyl chloroformate (4.3 mL, 33.3 mmol) at -20 °C under argon atmosphere. After being stirred for 30 min at 0 °C, the reaction mixture was filtered to remove the resulting precipitates. To a cooled suspension of sodium borohydride (2.5 g, 66.5 mmol) in water (30 mL) was added the filtrate at 0 °C. Stirring was continued for additional 30 min at the same temperature. The reaction mixture was diluted with EtOAc, washed with hydrochloric acid, water, brine, and dried over NaN-(tert-Butyloxycarbonyl)-O-Benzyl-L-Serinol (3)
Computed Properties
Molecular Weight:281.35
XLogP3:1.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:8
Exact Mass:281.16270821
Monoisotopic Mass:281.16270821
Topological Polar Surface Area:67.8
Heavy Atom Count:20
Complexity:282
Defined Atom Stereocenter Count:1
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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N-Boc-(S)-2-amino-3-benzyloxy-1-propanol
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