5-BROMO-1H-PYRROLO[2,3-B]PYRIDINE-3-CARBOXYLIC ACID
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![5-BROMO-1H-PYRROLO[2,3-B]PYRIDINE-3-CARBOXYLIC ACID structure](https://file.echemi.com/fileManage/upload/canonicalSmiles/20220812/cc44c3b1df9d4251935bb758554bbc30.png "5-BROMO-1H-PYRROLO[2,3-B]PYRIDINE-3-CARBOXYLIC ACID")
5-BROMO-1H-PYRROLO[2,3-B]PYRIDINE-3-CARBOXYLIC ACID
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CAS No:
849068-61-7
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Formula:
C8H5BrN2O2
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Chemical Name:
5-BROMO-1H-PYRROLO[2,3-B]PYRIDINE-3-CARBOXYLIC ACID
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Synonyms:
5-BROMO-1H-PYRROLO[2,3-B]PYRIDINE-3-CARBOXYLIC ACID;1H-Pyrrolo[2,3-b]pyridine-3-carboxylic acid, 5-bromo-;5-Bromo-7-azaindole-3-carboxylic acid;5-Bromo-7-azaindole-3-car...;3-b]pyridine-3-carboxylic acid;5-BroMo-7-azaindole-3-carboxylic
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CAS No:
Safety Information
IRRITANT
NONH for all modes of transport
3
22-36
26-24/25
Xi,Xn
P305 + P351 + P338
H302-H319
5-BROMO-1H-PYRROLO[2,3-B]PYRIDINE-3-CARBOXYLIC ACID Use and Manufacturing
5-Bromo-7-azaindole (10.00 g, 50.75 mmol)Was dissolved in dichloromethane (200 mL)Aluminum chloride (34.00 g, 254.99 mmol) was added, Stirred at room temperature for 10 minutes, Trichloroacetyl chloride (8.6 mL, 77 mmol) was added, Continue stirring at room temperature overnight, The reaction solution was poured into ice water, Filtration gave a white solid, The filtrate was extracted with ethyl acetate (200 mL x 3)Concentrate the filtered white solid, (250 mL) and water (125 mL) were added, triethylamine (50 mL) was added, stirred at room temperature for 24 h, The solvent was concentrated and evaporated to dryness, adjusted to pH 5-6 with 1.0 M dilute hydrochloric acid, filtered, dried at 50 ° C, The product was 8.20 g of an off-white solid, Yield: 67.0percent.
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5-BROMO-1H-PYRROLO[2,3-B]PYRIDINE-3-CARBOXYLIC ACID
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