5-BROMO-1,2,3,4-TETRAHYDRO-QUINOLINE HYDROCHLORIDE
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5-BROMO-1,2,3,4-TETRAHYDRO-QUINOLINE HYDROCHLORIDE
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CAS No:
114744-50-2
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Formula:
C9H11BrClN
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Chemical Name:
5-BROMO-1,2,3,4-TETRAHYDRO-QUINOLINE HYDROCHLORIDE
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Synonyms:
5-BROMO-1,2,3,4-TETRAHYDRO-QUINOLINE HYDROCHLORIDE;5-bromo-1,2,3,4-tetrahydroquinoline;5-BROMO-1,2,3,4-TETRAHYDRO-QUINOLINE1HCL SALT;5-bromo-1,2,3,4-tetrahydroquinoline HCl
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CAS No:
5-BROMO-1,2,3,4-TETRAHYDRO-QUINOLINE HYDROCHLORIDE Basic Attributes
248.54734
246.976334
DTXSID80551500
2933499090
5-BROMO-1,2,3,4-TETRAHYDRO-QUINOLINE HYDROCHLORIDE Use and Manufacturing
Compound e (1.05 g, 5 mmol) was dissolved in methanol (14 ml) and hydroxylamine hydrochloride (1.4 g, 20 mmol) was added and refluxed for 1 h.Concentrate in vacuo, add dichloromethane and 50percent NaHCO3 for 20 minutes, dry the organic layer and concentrate to a white solid. Yield: 99percent.The resulting white solid (5 mmol) was dissolved in methylene chloride (30 ml), cooled to 0 °C, AlH (Bu-i) 2 (20 ml, 30 mmol, 1.5 M in toluene) was slowly added, and the mixture was stirred for 30 min.Move to room temperature and stir overnight. Quenching with water under ice bath conditions, dichloromethane extraction, saturated brine, After drying over anhydrous sodium sulfate, it was concentrated and purified by silica gel column (PE:EA=3:1) to give 600 mg of pale yellow solid f, yield: 56.6percent.
Computed Properties
Molecular Weight:212.09
XLogP3:3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Exact Mass:210.99966
Monoisotopic Mass:210.99966
Topological Polar Surface Area:12
Heavy Atom Count:11
Complexity:138
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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5-BROMO-1,2,3,4-TETRAHYDRO-QUINOLINE HYDROCHLORIDE
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