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Home > Encyclopedia > 5-Methyl-2,3-pyridinedicarboxylic acid

5-Methyl-2,3-pyridinedicarboxylic acid

5-Methyl-2,3-pyridinedicarboxylic acid structure

5-Methyl-2,3-pyridinedicarboxylic acid 

structure
  • CAS No:

    53636-65-0

  • Formula:

    C8H7NO4

  • Chemical Name:

    5-Methyl-2,3-pyridinedicarboxylic acid

  • Synonyms:

    2,3-Pyridinedicarboxylic acid,5-methyl-;5-Methyl-2,3-pyridinedicarboxylic acid;5-Methylpyridine-2,3-dicarboxylic acid

Description

White or light yellow crystalline powder

5-Methyl-2,3-pyridinedicarboxylic acid Basic Attributes

181.15

181.15

611-023-6

2933399090

Characteristics

87.5

0.6

DryPowder; OtherSolid

1.5±0.1 g/cm3

436.2°C at 760 mmHg

217.6±28.7 °C

1.611

5-Methyl-2,3-pyridinedicarboxylic acid Use and Manufacturing

Methods of Manufacturing

The preparation method is based on 2-ethylacrolein, diethyl oxaloacetate and ammonium chloride as raw materials, reacting in the presence of ethanol solvent and catalyst, heating and refluxing for 5 hours, after cooling, adding water to wash twice, and then dewatering Layer, the organic phase is desolvated to obtain diethyl 5-ethyl-2, 3-pyridinedicarboxylate, which is further hydrolyzed in an acid medium to obtain a finished product.

Uses

5-Ethyl-2,3-pyridinedicarboxylic acid is an intermediate of the herbicide imazethapyr.

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