2,6-Dichloropurine
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2,6-Dichloropurine
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CAS No:
5451-40-1
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Formula:
C5H2Cl2N4
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Chemical Name:
2,6-Dichloropurine
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Synonyms:
9H-Purine,2,6-dichloro-;Purine,2,6-dichloro-;1H-Purine,2,6-dichloro-;2,6-Dichloro-9H-purine;2,6-Dichloropurine;2,6-Dichloro-1H-purine;NSC 18395;2,6-Dichloro-9H-purin;2,6-Dichloro-7H-purine;1839-23-2
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CAS No:
Characteristics
54.5
1.7
White to yellow Crystalline Powder
1.8±0.1 g/cm3
177 °C
405.4°C at 760 mmHg
231.3±9.3 °C
1.742
soluble
2-8°C
Safety Information
IRRITANT
NONH for all modes of transport
3
36/37/38-22
22-24/25-37/39-26-36
Xn,Xi
Irritant
Stable under normal temperatures and pressures.
P264, P270, P301+P310, P321, P330, P405, P501
H301
2,6-Dichloropurine Use and Manufacturing
To a solution of ZnCl2 (7.0 g, 110 mmol) in conc. hydrochloric acid(9.2 mL) at 10 °C was added finely powdered compound 4 (2.3 g, 13.6 mmol) with stirring. The resulting stirred mixture was cooledto 5 °C and added NaNO2 (1.27 g, 18.4 mmol) over a period of30 min keeping the temperature below 5 °C. The mixture wasstirred for additional 30 min and was diluted with 12 mL of water.The product was extracted with ethyl acetate (4 x 15 mL). Theorganic phase was washed with water (2 x 7 mL), dried overNa2SO4, and evaporated to dryness to yield 2.37 g (47percent) of finalcompound.
2,6-Dichloropurine is used in the synthesis of 2,6-diamino-substituted purine derivatives as potential cardiomyogenesis inducing agents.
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