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9-(Bromomethyl)anthracene

9-(Bromomethyl)anthracene structure

CAS No:
2417-77-8
Formula:
C15H11Br
Chemical Name:
9-(Bromomethyl)anthracene
Synonyms:
Anthracene,9-(bromomethyl)-;9-(Bromomethyl)anthracene;135195-16-3
Categories:
Pharmaceutical Intermediates > Bulk Drug Intermediates

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9-(Bromomethyl)anthracene Basic Attributes

Molecular Weight：

271.157

Exact Mass：

271.15

UNII：

9JN2QR4LWJ

DSSTox ID：

DTXSID70178881

HScode：

2903999090

Characteristics

PSA：

XLogP3：

5.3

Density：

1.4±0.1 g/cm3

Melting Point：

136-136.5 °C @ Solvent: Cyclohexane

Boiling Point：

411.7°C at 760 mmHg

Flash Point：

209.0±13.2 °C

Refractive Index：

1.728

Safety Information

Precautionary statement(s)：

P264, P270, P273, P301+P312, P330, P391, P501

Hazard Statements：

H302

GHS Classification：

|Warning|H302 (97.5%): Harmful if swallowed [Warning Acute toxicity, oral]|P264, P270, P273, P301+P312, P330, P391, and P501|Aggregated GHS information provided by 40 companies from 2 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.

9-(Bromomethyl)anthracene Use and Manufacturing

9-Bromomethylanthracene was prepared in good yield (>87percent) by the reduction of 9-anthracenecarboxaldehyde, followed by bromination with PBrA solution of triphenylphosphine (16.44 g, 100.8 mmol) in acetonitrile (120 mL) was flushed with nitrogen for 20 minutes. Bromine (3.3 mL) was added and a solution of anthracen-9-yl-methanol (15.0 g, 72.0 mmol) in acetonitrile (10O mL) was added dropwise. The mixture was stirred for 2 hours at room temperature and refrigerated at 57-(anthracen-9-ylmethoxy)-4-methyl-2H-chromen-2-one (48) SU06-02; 9-(bromomethyl)anthracene (47); To a stirring suspension of 9-anthracenemethanol (2.0 g, 9.6 mmol) at 0

Computed Properties

Molecular Weight:271.15
XLogP3:5.3
Rotatable Bond Count:1
Exact Mass:270.00441
Monoisotopic Mass:270.00441
Heavy Atom Count:16
Complexity:216
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

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Guide of 9-(Bromomethyl)anthracene

Basic Attributes
Characteristics
Safety Information
Use and Manufacturing
Computed Properties
Latest News
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9-(Bromomethyl)anthracene

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