1,2-Diethyl 1,2-hydrazinedicarboxylate
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1,2-Diethyl 1,2-hydrazinedicarboxylate
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CAS No:
4114-28-7
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Formula:
C6H12N2O4
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Chemical Name:
1,2-Diethyl 1,2-hydrazinedicarboxylate
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Synonyms:
1,2-Hydrazinedicarboxylic acid,1,2-diethyl ester;Bicarbamic acid,diethyl ester;1,2-Hydrazinedicarboxylic acid,diethyl ester;1,2-Diethyl 1,2-hydrazinedicarboxylate;s-Dicarbethoxyhydrazine;Diethyl bicarbamate;Diethyl hydrazodicarboxylate;Diethyl 1,2-hydrazinedicarboxylate;1,2-Bis(ethoxycarbonyl)hydrazine;sym-Dicarbethoxyhydrazine;1,2-Dicarbethoxyhydrazine;Ethyl hydrazoformate;N,N′-Diethoxycarbonylhydrazine;N,N′-Bis(ethoxycarbonyl)hydrazine;NSC 122715;NSC 17295;NSC 227421;NSC 3002;Hydrazodicarboxylic acid diethyl ester
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CAS No:
1,2-Diethyl 1,2-hydrazinedicarboxylate Basic Attributes
176.17
176.17
1781585
223-902-8
122715|227421|17295|3002
DTXSID6063307
2928000090
Characteristics
76.66000
0.67
1.324 g/cm3 @ Temp: -5 °C
135 °C
180 °C @ Press: 1 Torr
105.0±18.7 °C
1.446
1,2-Diethyl 1,2-hydrazinedicarboxylate Use and Manufacturing
Cool the mixture of 85% hydrazine hydrate and 95% ethanol to 10°C, add ethyl chloroformate and sodium carbonate solution dropwise with stirring, control the feeding speed, keep the ethyl chloroformate in excess, and add it before the sodium carbonate solution. , The feeding temperature is kept above 20℃. After feeding, continue to stir and react for 0.5h, filter out the precipitate, wash thoroughly with water and then vacuum dry at 80°C to obtain the finished product with a yield of 81-85%.
Organic synthesis intermediate.
1,2-Hydrazinedicarboxylic acid, 1,2-diethyl ester: INACTIVE
Computed Properties
Molecular Weight:176.17
XLogP3:0.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:176.07970687
Monoisotopic Mass:176.07970687
Topological Polar Surface Area:76.7
Heavy Atom Count:12
Complexity:142
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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