3,5-Dimethoxyphenylpropionic acid
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3,5-Dimethoxyphenylpropionic acid
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CAS No:
717-94-2
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Formula:
C11H14O4
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Chemical Name:
3,5-Dimethoxyphenylpropionic acid
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CAS No:
Safety Information
R36/37/38
26-36/37/39
Xi
P261, P264, P270, P271, P280, P301+P312, P302+P352, P304+P340, P305+P351+P338, P312, P321, P330, P332+P313, P337+P313, P362, P403+P233, P405, P501
H302
3,5-Dimethoxyphenylpropionic acid Use and Manufacturing
To a solution of 3-(3, 5-Dimethoxy-phenyl)-acrylic acid (12g, 57.7mmol) in EtOAc (100ml) and MeOH (100ml) was added carefully 10percent Pd/C (1.3g), the reaction mixture was shaken in Parr apparatus for 5hs under 30-40 psi of hydrogen, then the solution was passed through a celite pad, the filtrate was concentrated and dried at 5OTo a flame dried flask under argon was added Pd/C (10percent, 1 g) and ethanol (15 mL) to wet the palladium. A solution of [3- (3, 5-DIMETHOXYPHENYL)-2-PROPENOIC] acid (10 g, 48 [MMOL)] in ethanol was added slowly to the flask containing Pd/C under argon. A hydrogen balloon was connected to the flask and stirred under hydrogen for 16 h. The reaction was filtered through a [CELITE PLUG] and the filtrate was evaporated under vacuum. The residue was purified by Biotage to obtain [3- (3, ] 5- dimethoxyphenyl) propanoic acid (9.89 g, 47 [MMOL)] as a solid in 98percent [YIELD. 1H] NMR (CDCI3) [5] 2.7 (t, 2H), 2.9 (t, 2H), 3.8 (s, 6H), 6.4 (m, 3H); MS (ES) 211.0 (M+H) +.
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3,5-Dimethoxyphenylpropionic acid
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