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Aaron Mishkin

Precipitation titration with Volhard method

Becca Altic  Follow

Yes filtering is necessary as thiocyanate can complex the solid silver chloride per:

$$\ce{AgX_{(s)} + SCN-_{(aq)} -> Ag[SCN]X-_{(aq)}\tag{X = Cl, Br, I}}$$

This additional reaction requires more thiocyanate for back titration and thus gives a lower chloride concentration than is true.

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