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Alan Murrie

Titration of CH3COONa with HCl and pKa determination from half equivalence point

Bill Walker  Follow

When you titrate a base like ammonia (pKa of conjugate acid around 9.5) with hydrochloric acid, you can see that it buffers in the basic region and the equivalence point is in the acidic region:

enter image description here

When you try the same with acetate (pKa of conjugate acid around 4.8), if buffers in the acidic region, and the equivalence point is in the acidic region:

enter image description here(Sorry, bad copy and past job. The start of the curve should be in the basic region, with an initial sharp drop to the buffer region)

Here is a better graph, courtesy of EdV:

enter image description here

As you will find, it is difficult to distinguish the buffering region from the region past the equivalence point. Other than that, it is possible to do this, and there is nothing wrong with that.

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Erin Morano  Follow
I ran the titration curve for 0.1 M acetate ion solution versus 0.1 M HCl, in 0.01 mL acid increments. The titration curve is here: More
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Hugo Smith  Follow
Yeah, pretty easy to do the calculations. Nice that the pH at the half-equivalence point, at 12.5 mL added HCl, was the expected 4.74.More
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Joe Miller  Follow
chemistry.meta.stackexchange.com/a/4757/79678More
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Frank Hewes  Follow
Weird that the only upvote is from me. One thing I have noticed is that pH problems, including titration curves, tend not to get much love here. Oh well.More
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Joel Lui  Follow
. If you have any use for it, feel free to use it and annotate, etc., as you please. I did not bother to run the ammonia versus HCl, but it is trivial to do so. I upvoted, by the way. I will leave the figure up for a couple of days. Ignore the M-B stuff: it was for a physics SE comment.More
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