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Karen Simon

Which ether is formed by dehydration of propane-1,3-diol with sulfuric acid?

D. Sigdel  Follow

You could actually get a mixture of products,depending on what the concentration of the H2S04 is ; and whether it was used in excess.

If you drip propane-1,3-diol into the acid,the starting material will always be in low concentration,and this will favor intramolecular reaction leading to the cyclic dioxane (1,2-dioxycyclohexane).

If you add acid to the propane-1,3-diol. you get a mess of products ,including a little bit of the foregoing product,but also:

bis-dihydroxpropylether

1,3(di-hydroxypropoxy)propane

and various higher polymers

In some cases the diol might be oxidized to the dialdehyde or the dicarboxylic acid.

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Craig Dorschel  Follow

The equation for the dehydration of propane-1,3-diol with sulfuric acid is:

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Donald Werve  Follow

You could actually get a mixture of products,depending on what the concentration of the H2S04 is ; and whether it was used in excess.

If you drip propane-1,3-diol into the acid,the starting material will always be in low concentration,and this will favor intramolecular reaction leading to the cyclic dioxane (1,2-dioxycyclohexane).

If you add acid to the propane-1,3-diol. you get a mess of products ,including a little bit of the foregoing product,but also:

bis-dihydroxpropylether

1,3(di-hydroxypropoxy)propane

and various higher polymers

In some cases the diol might be oxidized to the dialdehyde or the dicarboxylic acid.

More

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