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+ Powders
+ Gelatin
+ Scanning electron microscopy
+ Scanning electrochemical microscopy
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Manoj Ranaweera

To visualize SEM structure of gelatin powder, is an accelerating...

Connor Smith  Follow

E-SEM can be an option

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Arjun Koli  Follow

I do not know which SEM you will be using. For a FESEM, as your sample is non-conducting, I feel that 20kV is very high. Without proper coating, lots of charging will happen at sample and it may even damage the sample. If you are using FESEM, I will suggest proper coating of a conducting material (Au coating) and then start with low voltage such as 3 or 5 kV and try to analyze your sample.
Hope this helps.

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Cramer Beasly  Follow

If your SEM is not too old (20+ years) 20 kV is too high for any observation. Use lower kV, much lower - not only to preserve you specimen, but to get better pictures of any specimen.
Observation of gelatin powder at low mags (less than 1000) should not be a problem (it should be coated). At higher mags it could be damaged, but you should try and see how hight in magnification you can go.

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Bhavesh  Follow

I aggree with the others before. Your sample will charge up quickly at 20KV. Also you will have to sputter Au or other metallic material on your powder to use an SEM anyway. The only exception would be an SEM capable of working under low pressure instead of vakuum. Then your non conductive sample might not load up so quickly, but in this case 20KV also seem to be very much to me.

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Arega Tayu  Follow

i2oKV is high value

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Astrophysics and Astronomy  Follow

I would hardly assume this. But it also depends on the entire energy of the beam, i.e. how big is the beam current. Therefore, watch whether the sample changes during imaging and slowly adapt the conditions. Gelatin often contains water which might affect the imaging conditions as well. 

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David Grisell  Follow

i mean to use normal SEM not FESEM


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