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Nancy Lubin

Water flow in condenser

Omar Hassan  Follow

Water should always enter from the bottom of a condenser (the end closest to the flask) and exit from the top of the condenser. Doing it this way always ensures that your condenser will be full of cooling water. If you set it up the opposite way, and if for some reason the rate of water flow into the condenser decreased and became slower than the rate of water exiting the condenser, then the condenser would not remain filled with water. If the reaction were unattended, this could cause problems. BTW, here is a link you might enjoy. It contains a lot of lab tips, including "how to hook up the water tubing to a condenser".

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Grace Vontobel  Follow
@Karl Gravity. If the flow come from the bottom, More
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Jose Castellanos  Follow
Yes, I thought that would be the case, but then I remembered counter current exchange and started to doubt.More
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Gary McAdam  Follow
@Karl "How should an empty space suddenly appear in the water? " If the top condenser connector is used as a water inlet, and if the inlet tubing falls off or otherwise fails, or if the water flow from the main is interrupted, then water will drain out the bottom condenser connector leaving the condenser jacket filled with only air.More
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Jonathan J Wilks  Follow
flow will fill the condenser; if it flows from the top, the water will tend to flow under gravity to the bottom and low flow will mean the coils/free space isnt full as the flow will be determined by the rate water flows out under gravity not the inherent flow rate of the water.More
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Jean Morris  Follow
the condenser if you hook it up the wrong way.More
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divine atheist  Follow

In general the cooling water is attached according to the countercurrent exchange mechanism to maximize the efficiency. Of course this doesn't work well for the Liebig condenser you pictured, but you generally wouldn't use this kind of condenser for reflux anyway. The most common condenser for reflux is the Dimroth condenser which can be used for countercurrent exchange without any problems as the entry and exit of the water are both at the top of the condenser.

Here is an image from Arbeitsmethoden in der organischen Chemie (page 43) that shows where to attach the cooling water for different condenser types.

enter image description here

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