3-phenyl-9H-carbazole
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3-phenyl-9H-carbazole
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CAS No:
103012-26-6
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Formula:
C18H13N
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Chemical Name:
3-phenyl-9H-carbazole
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Synonyms:
3-phenyl-9H-carbazole;3-phenylcarbazole;SCHEMBL321006;CHEMBL1173064;KS-00000LPK;MFCD22052094;ZINC34071153;AKOS027383982;OL10013;AK402264
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CAS No:
Safety Information
|Warning|H315 (100%): Causes skin irritation [Warning Skin corrosion/irritation]|P264, P280, P302+P352, P305+P351+P338, P321, P332+P313, P337+P313, and P362|The GHS information provided by 1 company from 1 notification to the ECHA C&L Inventory.
3-phenyl-9H-carbazole Use and Manufacturing
General procedure: Z1 (1 equivalent each), the corresponding donor molecule D-H (2.20 equivalents) and tribasic potassium phosphate (4.40 equivalents) are suspended under nitrogen atmosphere in DMSO and stirred at 100-120 C (20 h). Subsequently, the reaction mixture is poured into a saturated sodium chloride solution and the precipitate is filtered and washed with water. The solid is then dissolved in dichloromethane, dried over MgS04 and the solvent is evaporated under reduced pressure. The crude product is purified by recrystallization or by flash chromatography. The product is obtained as a solid.Compound A-4 (20.0 g, 51.8 mmol) prepared in Preparation Example A and In a nitrogen atmosphere, 2-bromodibenzo[b, e][1, 4] dioxine (30.0 g, 114.5 mmol) and Add 2-chloro-2 ', 6, 6'-triphenyl-4, 4'-bipyridine (41.9g, 0.1mol), 14.4 g (60 mmol) of Compound A-4 prepared in Preparation Example A (20.0 g, 51.8 mmol) and B-8-1 intermediate (22.0 g, 90.4 mmol), B-8-2 (31.1 g, 90.4 millimoles), sodium tert-butoxide (NaOtBu) (13.01 grams, 135.6 millimoles), Pd2 (dba) 3 (2.48 grams, 2.7 millimoles), and tri-tertiary butylphosphine (P (t -Bu) 3) (5.49 g, 50% in toluene) was added to xylene (300 ml), And the mixture was heated and refluxed under a stream of nitrogen for 12 hours.After removing the xylene therefrom, 200 ml of methanol was added thereto, The crystallized solid was filtered, dissolved in monochlorobenzene (MCB), and filtered through silica gel / diatomaceous earth.And then concentrated an appropriate amount of organic solvent therefrom to obtain compound B-8(32 grams, 64.3%).General procedure: A mixture of 10 mmol of the brominated complex, 12-20 mmol of the diarylamine or
Computed Properties
Molecular Weight:243.3
XLogP3:5.3
Hydrogen Bond Donor Count:1
Rotatable Bond Count:1
Exact Mass:243.104799419
Monoisotopic Mass:243.104799419
Topological Polar Surface Area:15.8
Heavy Atom Count:19
Complexity:307
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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