1,4-Bis(diphenylphosphino)butane-palladium(II) chloride
-
1,4-Bis(diphenylphosphino)butane-palladium(II) chloride
structure -
-
CAS No:
29964-62-3
-
Formula:
C28H28P2.Cl2Pd
-
Chemical Name:
1,4-Bis(diphenylphosphino)butane-palladium(II) chloride
-
Synonyms:
Dichloro-1,4-bis(diphenylphosphino)butane-palladium(II),Palladium(II)chloride1,4-bis(diphenylphosphino)butanecomplex;Dichloro[bis(1,4-diphenylphosphino)butane]palladium(II), Pd 17.6%;Palladium(ii)chloride1,4-b;1,4-Bis(diphenylphosphino)butane-palladium(II) chloride,98+%;Dichloro[1,4-bis(diphenylphosphino)butane]palladium (II) ,98%;4-Bis(diphenylphosphino)butane-palladiuM(II) chloride;1,4-Butylenebis(diphenylphosphine)-palladium dichloride;1,4- double(twophenyl phosphinebutane)twopalladiuM chloride
- Categories:
-
CAS No:
1,4-Bis(diphenylphosphino)butane-palladium(II) chloride Basic Attributes
603.8
602.007813
243-231-4
DTXSID30450296
28439000
Characteristics
0
7.41140
light-yellow Powder
285-305 °C
Soluble in ethanol, benzene, and ethereal solvents.
2.92E-11mmHg at 25°C
Safety Information
NONH for all modes of transport
3
36/37/38
24/25-36-27
Xn
P261, P264, P270, P271, P272, P280, P301+P312, P302+P352, P304+P312, P304+P340, P305+P351+P338, P312, P321, P330, P332+P313, P333+P313, P337+P313, P362, P363, P403+P233, P405, P501
H302
|Warning|H302 (14.29%): Harmful if swallowed [Warning Acute toxicity, oral]|P261, P264, P270, P271, P272, P280, P301+P312, P302+P352, P304+P312, P304+P340, P305+P351+P338, P312, P321, P330, P332+P313, P333+P313, P337+P313, P362, P363, P403+P233, P405, and P501|Aggregated GHS information provided by 7 companies from 3 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.
1,4-Bis(diphenylphosphino)butane-palladium(II) chloride Use and Manufacturing
Step one, adding 10 ml of sponge palladium (mixed with concentrated hydrochloric acid and concentrated nitric acid at a volume ratio of 3: 1), Until the sponge palladium completely dissolved to the dissolved solution by adding a percentage of concentration of 37percent concentrated hydrochloric acid to the solution is notThe filtrate was filtered while the brown nitroxide was retreated and the resulting filtrate was concentrated to a palladium palladium concentration of 0.5 g / mLAcid solution;Step 2: 44. Ogl, 4-bis (diphenylphosphino) butane was added to 400 mL of N, N-dimethylformamide, heatedTo 50 ° C to give a solution of bis (diphenylphosphino) alkane in N, N-dimethylformamide;[0030] Step 3: To a solution of N, N-dimethylformamide in bis (diphenylphosphino) alkane as described in step 2 under stirringThe solution of the chloropalladic acid in step 1 was added dropwise, and the reaction was carried out under the condition of stirring at a temperature of 50 ° C for 60 min.After the reaction solution is cooled and filtered to obtain a filter cake;[0031] Step 4: Wash the filter cake in step 3 with absolute ethanol, and then, at a temperature of 50 ° C, 0. 06 MPa, the dried filter cake was vacuum dried for 4 h to give a pale yellow powder of 1, 4-bis (diphenylphosphino) butane diPalladium chloride complex (C2SH2SCl2P2Pd) 56. lg, yield 98.9percent.
Coupling catalyst
Computed Properties
Molecular Weight:603.8
Rotatable Bond Count:9
Exact Mass:602.00781
Monoisotopic Mass:602.00781
Heavy Atom Count:33
Complexity:364
Covalently-Bonded Unit Count:2
Compound Is Canonicalized:Yes
Recommended Suppliers of 1,4-Bis(diphenylphosphino)butane-palladium(II) chloride
-
![China]()
CN
5 YRS
Business licensedTrader Supplier of Intermediates,Building blocks,API,Silicones,Peptides,Lab chemicals,Biochemicals,Pharmaceuticals,Screening Compounds,Food Additives -
![China]()
CN
5 YRS
Business licensed Certified factoryManufactory Supplier of Active Pharm Ingredients,Chemical Catalyst,Pharmaceutical Intermediates,Flavors and Fragrances,Agrochemicals,Chemical Pesticides,Organic Intermediates,OLED IntermediatesInquiryCAS No.: 29964-62-3Grade: Industrial GradeContent: 99% -
![China]()
CN
5 YRS
Business licensedTrader Supplier of PVC resin,pvc paste resin,melamineInquiryCAS No.: 29964-62-3Grade: Industrial GradeContent: 99%
Learn More Other Chemicals
-
1,3,5-Cycloheptatriene-1-carbonyl chloride (9CI)
103533-75-1
-
3'-De(diMethylaMino)-3'-[[(2-Methoxyethoxy)Methyl]diMethylaMMonio]erythroMycin 9-OxiMe Chloride
151750-47-9
-
decoxymethyl-dimethyl-octyl-azanium chloride
366491-03-4
-
4-[3-(3,5-DICHLORO-PHENYL)-UREIDO]-BENZENESULFONYL CHLORIDE Formula
677326-84-0
-
2,5-DICHLOROBENZYLZINC CHLORIDE Formula
737797-20-5
-
2,5-DIBROMO-3,6-DIFLUOROBENZENESULFONYL CHLORIDE Formula
207853-66-5
-
Dibenzofuran-3-sulfonyl chloride Structure
42138-14-7
-
2,4-Dibromo-5-fluorobenzenesulfonyl chloride Structure
1000578-09-5
-
What is Selenium(I) chloride (99%-Se)
21317-32-8
-
What is 2,6-dibromo-4-methylbenzene-1-sulfonyl chloride
73732-31-7
1,4-Bis(diphenylphosphino)butane-palladium(II) chloride
SDSRequest for Quotation