4-Bromo-5-fluoro-2-nitrobenzoic acid
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4-Bromo-5-fluoro-2-nitrobenzoic acid
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CAS No:
1020717-99-0
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Formula:
C7H3BrFNO4
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Chemical Name:
4-Bromo-5-fluoro-2-nitrobenzoic acid
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Synonyms:
Benzoic acid,4-bromo-5-fluoro-2-nitro-;4-Bromo-5-fluoro-2-nitrobenzoic acid
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CAS No:
Safety Information
P261, P264, P271, P280, P302+P352, P304+P340, P305+P351+P338, P312, P321, P332+P313, P337+P313, P362, P403+P233, P405, P501
H315
4-Bromo-5-fluoro-2-nitrobenzoic acid Use and Manufacturing
Compound 1 (75 g, 342.5 mmol) was dissolved in sulfuric acid (500 ml) at room temperature, and nitric acid (103.8 g, 1027 mmol) was added slowly. After stirring for 18 h, the mixture was slowly poured over 3 kg of ice, stirred, filtered, washed with water and dried at 45 ° C under reduced pressure to give compound 2 (90 g, 99.5percent).To a solution of 4-bromo-3-fluorobenzoic acid (20 g, 91 mmol) in concentrated H
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4-Bromo-5-fluoro-2-nitrobenzoic acid
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