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2-Bromo-1,3-dichlorobenzene

2-Bromo-1,3-dichlorobenzene structure

CAS No:
19393-92-1
Formula:
C6H3BrCl2
Chemical Name:
2-Bromo-1,3-dichlorobenzene
Synonyms:
Benzene,2-bromo-1,3-dichloro-;2-Bromo-1,3-dichlorobenzene;1,3-Dichloro-2-bromobenzene;2,6-Dichlorobromobenzene;1-Bromo-2,6-dichlorobenzene;NSC 155332
Categories:
Organic Chemistry > Hydrocarbons and Derivatives

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Description

white to light yellow crystal powder

2-Bromo-1,3-dichlorobenzene Basic Attributes

Molecular Weight：

225.9

Exact Mass：

225.90

BRN：

1681054

EC Number：

243-018-6

NSC Number：

155332

DSSTox ID：

DTXSID00173006

HScode：

29039990

Characteristics

PSA：

XLogP3：

3.9

Appearance：

White to yellow Crystalline Powder and/or Chunks

Density：

1.6351 (rough estimate)

Melting Point：

65 °C

Boiling Point：

242 °C

Flash Point：

>100°C

Refractive Index：

1.5700 (estimate)

Vapor Pressure：

0.0549mmHg at 25°C

Safety Information

Transport codes：

NONH for all modes of transport

wgk germany：

hazard class code：

36/37/38

safety instructions：

26-37/39-28A

Marks：

Hazard note：

Irritant

Precautionary statement(s)：

P261-P305 + P351 + P338

Hazard Statements：

H315-H319-H335

GHS Classification：

|Warning|H315 (100%): Causes skin irritation [Warning Skin corrosion/irritation]|P261, P264, P271, P280, P302+P352, P304+P340, P305+P351+P338, P312, P321, P332+P313, P337+P313, P362, P403+P233, P405, and P501|Aggregated GHS information provided by 134 companies from 5 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.

2-Bromo-1,3-dichlorobenzene Use and Manufacturing

4-Bromo-3, 5-dichlorophenol (11): The general process was applied to a solution of The solution of 2-bromo-1 , 3-dichlorobenzene (13 g, 58 mmol), 2, 2-dimethyl-2-silabut- 3-yne (90 mL, 64 mmol), CuI (100 mg, 5.5 mmol), PPh3 (200 mg, 0.75 mmol) and Pd(PPh3)2Cl2 (235 mg, 0.335 mmol) in 35 mL of NEt3 was refluxed in a seal tube under N2 atmosphere for 24 h. Both of TLC and LCMS indicated that the reaction was over. Concentrated and EtOAc was added. The solution was washed with water and brine, dried over Na2SO*, filtered, concentrated and purified by flash chromatography on silica gel (eluent: PE/EA = 100/0) to give 13 g of crude compound A1f as an oil (yield 40percent, purity 70percent).

Computed Properties

Molecular Weight:225.89
XLogP3:3.9
Exact Mass:223.87952
Monoisotopic Mass:223.87952
Heavy Atom Count:9
Complexity:87.1
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

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2,6-Dichlorobromobenzene

CAS No.: 19393-92-1

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1-BROMO-2,6-DICHLOROBENZENE,CAS 19393-92-1

CAS No.: 19393-92-1

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Guide of 2-Bromo-1,3-dichlorobenzene

Description
Basic Attributes
Characteristics
Safety Information
Use and Manufacturing
Computed Properties
Recommended Suppliers
Latest News
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2-Bromo-1,3-dichlorobenzene

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