Hydrazine, (2,6-dichlorophenyl)-, hydrochloride (1:1)
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Hydrazine, (2,6-dichlorophenyl)-, hydrochloride (1:1)
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CAS No:
50709-36-9
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Formula:
C6H6Cl2N2.ClH
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Chemical Name:
Hydrazine, (2,6-dichlorophenyl)-, hydrochloride (1:1)
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Synonyms:
Hydrazine,(2,6-dichlorophenyl)-,hydrochloride (1:1);Hydrazine,(2,6-dichlorophenyl)-,monohydrochloride;2,6-Dichlorophenylhydrazine hydrochloride
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CAS No:
Hydrazine, (2,6-dichlorophenyl)-, hydrochloride (1:1) Basic Attributes
213.49
211.967484
4569738
256-730-7
29280000
Characteristics
38
1.6100 (rough estimate)
218 °C (decomp)
253.5°C at 760 mmHg
107.1ºC
Room temperature.
Safety Information
I; II; III
6.1
UN 2811 6.1/PG 3
3
20/21-25-36/37/38-20/21/22
26-36/37/39-45-22
T,Xi,Xn
Irritant
P261-P280-P301 + P310-P305 + P351 + P338
H301-H312 + H332-H315-H319-H335
Hydrazine, (2,6-dichlorophenyl)-, hydrochloride (1:1) Use and Manufacturing
To a cold solution of 2, 6-dichloroaniline (10.0 g, 61.72 mmol) in cone. HCl was added aqueous solution of sodium nitrite (5.1 1 g, 74.00 mmol) at -15°C. The reaction mass was stirred at 0-10°C for 15 minutes. The reaction mass was filtered off to remove insolubles and stannous chloride in cone. HC1 (34.7 g, 150 mmol) was added to the filtrate. The reaction mass was further stirred at -15°C for 30 min and filtered to afford 15.00 g of the desired product. A mixture of compound P9-3 (5.1 g, 20 mmol) and
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