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Methyl 4-nitro-L-phenylalaninate hydrochloride

Methyl 4-nitro-L-phenylalaninate hydrochloride structure

CAS No:
17193-40-7
Formula:
C10H12N2O4.ClH
Chemical Name:
Methyl 4-nitro-L-phenylalaninate hydrochloride
Synonyms:
L-Phenylalanine,4-nitro-,methyl ester,hydrochloride (1:1);Alanine,3-(p-nitrophenyl)-,methyl ester,monohydrochloride,L-;L-Phenylalanine,4-nitro-,methyl ester,monohydrochloride;p-Nitrophenylalanine methyl ester hydrochloride;Methyl 4-nitro-L-phenylalaninate hydrochloride;(S)-1-Methoxycarbonyl-2-(4-nitrophenyl)ethanaminium chloride;(S)-2-Amino-3-(4-nitrophenyl)propionic acid methyl ester hydrochloride;Methyl (S)-2-amino-3-(4-nitrophenyl)propanoate hydrochloride
Categories:
Biochemical Engineering > Amino Acids and Derivatives

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Description

White solid

Methyl 4-nitro-L-phenylalaninate hydrochloride Basic Attributes

Molecular Weight：

260.67

Exact Mass：

260.056396

BRN：

5176380

EC Number：

605-624-2

HScode：

29225090

Characteristics

PSA：

98.1

XLogP3：

2.66310

Melting Point：

210-214 °C

Boiling Point：

360ºC at 760 mmHg

Flash Point：

171.5ºC

Storage Conditions：

2-8°C

Vapor Pressure：

2.29E-05mmHg at 25°C

Safety Information

Packing level：

III

Hazard category：

6.1

Transport codes：

2811

wgk germany：

hazard class code：

22-43-36

safety instructions：

22-36/37-24/25

Precautionary statement(s)：

P261, P264, P272, P280, P302+P352, P305+P351+P338, P321, P333+P313, P337+P313, P363, P501

Hazard Statements：

H317

Methyl 4-nitro-L-phenylalaninate hydrochloride Use and Manufacturing

Thionyl chloride (1.03 ml, 14.2 mmol) was added dropwise to a suspension of L-p- Nitrophenylalanine (0.995 g, 4.73 mmol) in 10 ml of MeOH at 0°C. After the addition, the solution formed was allowed to warm to room temperature. The reaction mixture was heated under reflux overnight and then concentrated. The crude material was recrystallized from methanol/ethyl acetate to give 1.012 g (95percent) of L-p-Nitrophenylalanine Methyl Ester Hydrochloride.SOCl(2) The above product was dissolved in 20 mL of saturated anhydrous methanol and hydrogenated for 15 min, and refluxed at room temperature for 4 h.The solid was collected by dryness to give 8.5 g of methyl 2-amino-3-methyl-4-amino-3-(4-nitrophenyl)chloropropionate (methyl 2-amino-3-methyl).(4-nitrophenyl)propanoate hydrochloride).

Recommended Suppliers of Methyl 4-nitro-L-phenylalaninate hydrochloride

HANGZHOU LEAP CHEM CO., LTD. Contact Supplier

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L-4-Nitrophenylalanine methyl ester hydrochloride

CAS No.: 17193-40-7

Content: 99.00%

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shanghai jinghui industrial co.ltd Contact Supplier

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L-4-Nitrophenylalanine methyl ester hydrochloride 99% colorless liquid JINGHUI

CAS No.: 17193-40-7

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Guide of Methyl 4-nitro-L-phenylalaninate hydrochloride

Description
Basic Attributes
Characteristics
Safety Information
Use and Manufacturing
Recommended Suppliers
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Methyl 4-nitro-L-phenylalaninate hydrochloride

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