D-Alanine, methyl ester, hydrochloride
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D-Alanine, methyl ester, hydrochloride
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CAS No:
14316-06-4
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Formula:
C4H9NO2.ClH
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Chemical Name:
D-Alanine, methyl ester, hydrochloride
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Synonyms:
D-Alanine,methyl ester,hydrochloride (1:1);Alanine,methyl ester,hydrochloride,D-;D-Alanine,methyl ester,hydrochloride;Methyl D-alaninate hydrochloride;(R)-2-Aminopropionic acid methyl ester hydrochloride;(R)-Alanine methyl ester hydrochloride;NSC 523192;(R)-1-(Methoxycarbonyl)ethylamine hydrochloride;Methyl (R)-2-aminopropanoate hydrochloride;(R)-Methyl 2-aminopropanoate hydrochloride
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CAS No:
Characteristics
52.3
0.43460
White to off-white Crystalline Powder
1.01g/cm3
95-97 °C
101.5ºC at 760 mmHg
Soluble in Water 100 mg/ml.
2-8°C
35mmHg at 25°C
-8 º (c=1.6, MeOH)
D-Alanine, methyl ester, hydrochloride Use and Manufacturing
General procedure: SOClIn a separate reaction, the intermediate reagent V(E) was prepared by suspending V(D) (100 g, 1.12 mol) in 1 L of MeOH. The mixture was cooled to 0-5 D-alanine (2.5 g, 27.8 mmol) was added to a dry flask.Add anhydrous anaerobic methanol (14 mL), stir at 20 ° C for 10 min, Thionyl chloride (5 mL) was slowly added thereto, and the reaction was stirred for 6 hours.After the reaction was completed, the solvent was evaporated, diluted with diethyl ether and filtered.D-Alanine methyl ester 9 was obtained as a white solid, 3.46 g.
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D-Alanine, methyl ester, hydrochloride
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