FMOC-PHE-OL
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FMOC-PHE-OL
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CAS No:
129397-83-7
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Formula:
C24H23NO3
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Chemical Name:
FMOC-PHE-OL
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Synonyms:
N-FMOC-L-PHENYLALANINOL;N-ALPHA-FMOC-L-PHENYLALANINOL;N-(9-FLUORENYLMETHOXYCARBONYL)-L-PHENYLALANINOL;FMOC-L-PHENYLALANINOL;FMOC-PHENYLALANINOL;FMOC-PHE-OL;FMOC-(S)-2-AMINO-3-PHENYL-1-PROPANOL;Fmoc-DL-Phenylalaninol
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CAS No:
Characteristics
58.6
4.4
Solid
1.219±0.06 g/cm3(Predicted)
129-130 °C
606.1±50.0 °C(Predicted)
300.2±30.1 °C
1.659
-15°C
1.52E-15mmHg at 25°C
FMOC-PHE-OL Use and Manufacturing
General procedure: To a solution of carboxylic acid (10 mmol) in THF (10 mL), DIPEA (11 mmol, 1.42 mL) and 50percent T3P in EtOAc (20 mmol, 6.36 mL) were added at 0 °C and the solution was stirred for about 10 min. Then aqueous solution of NaBHGeneral procedure: Amine (1 mmol) and Fmoc-Cl (1.1 mmol) were placed in a glass tube under neat conditions and were sonicated for a suitable time (as indicated in Tables 1, 2 and 3). All reactions were performed in a water bath at room temperature. After completion of the reaction (as indicated by TLC), 5 cm3 of diethyl ether was added to the mixture. The N-Fmoc derivatives were crystallized and were obtained in good to excellent yields. Purification of the product was accomplished by recrystallization from diethyl ether.
Computed Properties
Molecular Weight:373.4
XLogP3:4.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:373.16779360
Monoisotopic Mass:373.16779360
Topological Polar Surface Area:58.6
Heavy Atom Count:28
Complexity:482
Defined Atom Stereocenter Count:1
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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