β-D-Mannopyranose, 1,3,4,6-tetraacetate
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β-D-Mannopyranose, 1,3,4,6-tetraacetate
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CAS No:
18968-05-3
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Formula:
C14H20O10
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Chemical Name:
β-D-Mannopyranose, 1,3,4,6-tetraacetate
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Synonyms:
β-D-Mannopyranose,1,3,4,6-tetraacetate;Mannopyranose,1,3,4,6-tetraacetate,β-D-;1,3,4,6-Tetra-O-acetyl-β-D-mannopyranose
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CAS No:
Characteristics
135
0.1
1.259g/cm3
160-161 °C(lit.)
425.537°C at 760 mmHg
79.1ºC
-22.5 ° (C=1.4, CHCl3)
Refrigerator
β-D-Mannopyranose, 1,3,4,6-tetraacetate Use and Manufacturing
To a solution of the orthoester4(4.4 g, 12 mmol) in anhydrous acetone (27 mL) was added 1M hydrochloric acid (HCl) aq. (2.7 mL) in one portion with vigorous stirring (~18°C, water bath). After being stirred for an additional 5 min at room temperature, the reaction mixture was concentrated on a rotary evaporator below 20°C. The resulting solid was dissolved in CHClTo a solution of compound 10 (11.24 g, 30 mmol) in acetone (40 ml), 1M HCl (aq) was added in one portion while vigorously stirring in a water bath. The mixture was stirred at room temperature for 10 min. It was then concentrated under reduced pressure. CHCl
An intermediate in the preparation of precursors of 2-[18F]fluoro-2-deoxy-D-glucose for diagnostic use in positron emission tomography.
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