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L-Pyroglutamamide

L-Pyroglutamamide structure

L-Pyroglutamamide 

structure

L-Pyroglutamamide Basic Attributes

128.13

128.058578

DTXSID80332159

2933790090

Characteristics

72.2

-1.4

1.285±0.06 g/cm3(Predicted)

148-150 °C(Solv: methanol (67-56-1))

515.9±39.0 °C(Predicted)

265.8±27.1 °C

1.515

L-Pyroglutamamide Use and Manufacturing

General procedure: Stirred L-pyroglutamic acid methyl ester (10 mmol) in NH3 [aq]/N2H4 [aq] (50 mL) for 12 h at room temperature. Then the mixture was allowed to stand for one day at −10 °C. Next the crystallization washed with ethanol, ether, dried over MgSO4, The crude mixture was purified by flash column chromatography on silica (MeOH/CH2Cl2=1/6) to provide pure product as white solid.

Computed Properties

Molecular Weight:128.13
XLogP3:-1.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:128.058577502
Monoisotopic Mass:128.058577502
Topological Polar Surface Area:72.2
Heavy Atom Count:9
Complexity:155
Defined Atom Stereocenter Count:1
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

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