D-Phenylglycine methyl ester hydrochloride
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D-Phenylglycine methyl ester hydrochloride
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CAS No:
19883-41-1
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Formula:
C9H11NO2.ClH
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Chemical Name:
D-Phenylglycine methyl ester hydrochloride
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Synonyms:
Benzeneacetic acid,α-amino-,methyl ester,hydrochloride (1:1),(αR)-;Glycine,2-phenyl-,methyl ester,hydrochloride,D-;Benzeneacetic acid,α-amino-,methyl ester,hydrochloride,(R)-;Benzeneacetic acid,α-amino-,methyl ester,hydrochloride,(αR)-;Methyl D-phenylglycinate hydrochloride;D-Phenylglycine methyl ester hydrochloride;D-α-Aminophenylacetic acid methyl ester hydrochloride;Methyl D-α-phenylglycine hydrochloride;Methyl (R)-phenylglycinate hydrochloride;(R)-Phenylglycine methyl ester hydrochloride;Methyl D-α-phenylglycinate hydrochloride;(R)-(-)-2-Phenylglycine methyl ester hydrochloride;((R)-2-Methoxy-2-oxo-1-phenylethyl)ammonium chloride;(R)-Methyl 2-amino-2-phenylacetate hydrochloride;Methyl (R)-amino(phenyl)acetate hydrochloride;(R)-Methyl 2-amino-2-phenylacetate hydrochloride;(R)-2-Phenylglycine methyl ester hydrochloride;Methyl (R)-2-amino-2-phenylacetate hydrochloride;40860-96-6
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CAS No:
D-Phenylglycine methyl ester hydrochloride Basic Attributes
201.65
201.055649
3915654
243-399-9
29224999
Characteristics
52.3
1.126g/cm3
198-201 °C @ Solvent: Diethyl ether, Methanol
238.9°C at 760 mmHg
104.7ºC
2-8°C
-118o (C=1 IN H2O)
D-Phenylglycine methyl ester hydrochloride Use and Manufacturing
General procedure: The methyl-esterification reaction of L-phenylalanine.To a suspension of L-phenylalanine (1 g, 6.05 mmol, 1.0 equiv) inmethanol (25 mL) cooled to 0 C was added thionyl chloride(475 mL, 6.66 mmol, 1.5 equiv) slowly. After 10 min, the reactionmixture was heated to 75 C to reflux for 2 h. After completion(monitored by TLC), the solvent was removed in vacuo, and at thistime, a white solid was formed methyl L-phenylalaninate hydrochloride(1.23 g, quantitative yield).
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D-Phenylglycine methyl ester hydrochloride
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