N-Benzyloxycarbonyl-N'-(tert-Butoxycarbonyl)-L-lysine
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N-Benzyloxycarbonyl-N'-(tert-Butoxycarbonyl)-L-lysine
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CAS No:
66845-42-9
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Formula:
C19H28N2O6
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Chemical Name:
N-Benzyloxycarbonyl-N'-(tert-Butoxycarbonyl)-L-lysine
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Synonyms:
NALPHA-BENZYLOXYCARBONYL-NOMEGA-TERT-BUTOXYCARBONYL-D-LYSINE;N-BENZYLOXYCARBONYL-N-EPSILON-TERT-BUTOXYCARBONYL-L-LYSINE;N-ALPHA-CBZ-N-EPSILON-BOC-D-LYSINE;N-ALPHA-CBZ-N-EPSILON-T-BOC-D-LYSINE;N-ALPHA-CBZ-N-EPSILON-T-BOC-L-LYSINE;N-ALPHA-CARBOBENZOXY-N-EPSILON-T-BUTOXYCARBONYL-D-LYSINE;N-ALPHA-CARBOBENZOXY-N-EPSILON-T-BUTOXYCARBONYL-L-LYSINE;N-ALPHA-Z-N-EPSILON-BOC-D-LYSINE
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CAS No:
N-Benzyloxycarbonyl-N'-(tert-Butoxycarbonyl)-L-lysine Use and Manufacturing
(4 g, 10.5 mmol) and methyl4-N-BOC-piperidin-4-carboxylate (3 g, 5.0 mmol) were dissolved in dichloromethane (10 mL), and the resultant mixture was cooled to 0 C. Under the protection of nitrogen, DIEA (5.43 g, 42 mmol), copper dichloride dehydrate (1.88 g, 11 mmol), HOBt(1.62 g, 12 mmol), and HBTU (4.55g, 12 mmol) were separately added. The reaction was carried out for 16 h. The title compound (a crude product, 6.69g) was obtained after workup, amd was used directly in the next step. ESI-MS (m/z): 621(M+H)+;
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N-Benzyloxycarbonyl-N'-(tert-Butoxycarbonyl)-L-lysine
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