N-[(Phenylmethoxy)carbonyl]-L-norvaline
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N-[(Phenylmethoxy)carbonyl]-L-norvaline
structure -
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CAS No:
21691-44-1
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Formula:
C13H17NO4
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Chemical Name:
N-[(Phenylmethoxy)carbonyl]-L-norvaline
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Synonyms:
L-Norvaline,N-[(phenylmethoxy)carbonyl]-;Norvaline,N-carboxy-,N-benzyl ester,L-;N-[(Phenylmethoxy)carbonyl]-L-norvaline;N-(Benzyloxycarbonyl)-L-norvaline;N-(Carbobenzoxy)norvaline;(Benzyloxycarbonyl)norvaline;N-(Benzyloxycarbonyl)norvaline;L-(Carbobenzyloxy)norvaline;Z-L-Norvaline;N-Carbobenzyloxy-L-norvaline;Cbz-L-norvaline;(2S)-2-(Phenylmethoxycarbonylamino)pentanoic acid
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CAS No:
Characteristics
75.6
2.3
1.2±0.1 g/cm3
439.4°C at 760 mmHg
219.6±26.8 °C
1.533
Store at RT.
1.69E-08mmHg at 25°C
N-[(Phenylmethoxy)carbonyl]-L-norvaline Use and Manufacturing
Compound vii (15.39 g, 32.1 mmol) from step a was charged into THF (100 mL) and 1N HCl (50 mL). The resulting emulsion was stirred overnight at the room temperature and then concentrated under vacuum to provide a thick oil. The oil was then dissolved in THF (100 mL), and to the solution was added water (25 mL) and LiOH (3.08 g, 128 mmol). This solution was stirred overnight again at the room temperature and then concentrated to remove THF. A hazy light yellow emulsion remained. This was diluted with water (25 mL) and extracted with CH
Biochemical research
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N-[(Phenylmethoxy)carbonyl]-L-norvaline
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