L-Isoleucine, methyl ester, hydrochloride (1:1)
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L-Isoleucine, methyl ester, hydrochloride (1:1)
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CAS No:
18598-74-8
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Formula:
C7H15NO2.ClH
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Chemical Name:
L-Isoleucine, methyl ester, hydrochloride (1:1)
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Synonyms:
L-Isoleucine,methyl ester,hydrochloride (1:1);Isoleucine,methyl ester,hydrochloride,L-;L-Isoleucine,methyl ester,hydrochloride;Methyl isoleucinate hydrochloride;Isoleucine methyl ester hydrochloride;Methyl L-isoleucinate hydrochloride;259795-94-3;660838-98-2;1172585-50-0;1315562-13-0;1396967-40-0;1416477-68-3;1537871-99-0;1631128-49-8;1936458-88-6
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CAS No:
L-Isoleucine, methyl ester, hydrochloride (1:1) Basic Attributes
181.66
181.086960
3595132
242-437-1
29224999
Characteristics
52.3
2.03510
Off-white to orange Powder or Crystalline Powder
0.955g/cm3
100.5-101 °C
169.2ºC at 760mmHg
42.7ºC
26.5 ° (C=2, H2O)
Soluble in methanol (50 mg/ml clear, colorless solution).
0-6°C
1.56mmHg at 25°C
27 º (c=2% in H2O)
Safety Information
IRRITANT
NONH for all modes of transport
3
36/37/38-40
26-36/37/39-36-22-24/25
Xi,Xn
L-Isoleucine, methyl ester, hydrochloride (1:1) Use and Manufacturing
General procedure: To 5 mL of ice-bath cooled methanol was added dropwise 1 mL of SOClGeneral procedure: This compound has previously been describedMethanol (12.5 mL) was placed in a reaction flask and cooled to 10 °C. Thionyl chloride (2.5 mL, 35 mmol) was added dropwise to the stirred methanol for 10 minutes. L-Isoleucine (1.0 g, 7.7 mmol) was added to the reaction mixture at once and stirred for 2 days at room temperature. After removal of the solvent, methanol was added to the crude material and evaporated. This step was repeated twice to remove the residual thionyl chloride. The resulting solid was purified by column chromatography on silica gel (30 g, CHCl
Used in biochemical reagents and pharmaceutical intermediates.
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L-Isoleucine, methyl ester, hydrochloride (1:1)
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