6-Amino-3-methyluracil
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6-Amino-3-methyluracil
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CAS No:
21236-97-5
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Formula:
C5H7N3O2
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Chemical Name:
6-Amino-3-methyluracil
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Synonyms:
6-Amino-3-methyluracil ,97%;3-Methyl-6-aMinouracil;6-Amino-3-methyl-1H-pyrimidine-2,4-dione;6-Amino-3-methylpyrimidine-2,4(1H,3H);6-amino-3-methyldihydropyrimidine-2,4(1H,3H)-dione
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CAS No:
6-Amino-3-methyluracil Use and Manufacturing
6-Aminouracil (5) (5.18 g, 40.7 mmol) was suspended in HM DS (25 mL) and HStep 1 6-amino-3-methylpyrimidine-2, 4(lH, 3H)-dione To a solution of the 6-aminopyrimidine-2, 4(lH, 3H)-dione (15 g, 1 18 mmol) in 1 , 1 , 1 , 3, 3, 3- hexamethyldisilazane (50 mL) was added ammonium sulfate(0.671g, 5 mmol), then the resulting mixture was heated to reflux with stirring for 6 h. The mixture was concentrated to give a light-yellow solid. This solid was combined with acetonitrile (50 mL) and iodomethane (15 mL, 250 mmol) was added. The resulting mixture was stirred at 40 °C for 16 h. Then the mixture was concentrated, neutralized with saturated sodium bicarbonate to pH =7, filtered, and the filter cake was washed with brine and ethanol, dried under vacuum to give 6-amino-3- methylpyrimidine-2, 4 (lH, 3H)-dione (7.1 g, 42.6 percent yield) as yellow solid. LCMS MH
Computed Properties
Molecular Weight:141.13
XLogP3:-1.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Exact Mass:141.053826475
Monoisotopic Mass:141.053826475
Topological Polar Surface Area:75.4
Heavy Atom Count:10
Complexity:221
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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