Benzaldehyde, 4-(ethylamino)- (9CI)

A mixture of an 4-fluorobenzaldehyde (12.4 g, 0.1 mol), 60percent aqueous ethylamine solution (50 mL, 0.67 mol), and a stirring bar was sealed in a 100 mL autoclave and stirred electromagnetically in an oil bath at 130 °C for 15 h [23, 24]. The mixture was extracted with ethyl acetate for 3 times (50 mL × 3), combined organic extracts and washed by 10percent hydrochloric acid twice (50 mL × 2). The pH of the aqueous phase was adjusted to 9 by 10percent sodium carbonate solutions. The aqueous phase was extracted with ethyl acetate for 3 times (30 mL × 3), combined organic extracts and dried with NaSOGeneral procedure: To a solution of p-fluoro benzaldehyde (1 equiv.), tetrabutylammonium bromide (0.3 equiv.) and the appropriate amine (1.5 equiv.) in DMSO, K

Molecular Weight:149.19
XLogP3:1.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:149.084063974
Monoisotopic Mass:149.084063974
Topological Polar Surface Area:29.1
Heavy Atom Count:11
Complexity:117
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes