2-BROMOMETHYL-1-METHYL-4-NITRO-BENZENE
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2-BROMOMETHYL-1-METHYL-4-NITRO-BENZENE
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CAS No:
98799-27-0
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Formula:
C8H8BrNO2
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Chemical Name:
2-BROMOMETHYL-1-METHYL-4-NITRO-BENZENE
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Synonyms:
2-(Bromomethyl)-1-methyl-4-nitrobenzene;2-Bromomethyl-1-methyl-4-nitrobenzene;Benzene, 2-(bromomethyl)-1-methyl-4-nitro-;SCHEMBL694999;BEN301;2-Methyl-5-nitrobenzyl bromide;CTK8F4159;DTXSID60679433;ZINC44137808;AK-83225
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CAS No:
2-BROMOMETHYL-1-METHYL-4-NITRO-BENZENE Use and Manufacturing
General procedure: Adapting literature known protocols (Harrison and Diehl, Org. Synth., 1955, Coll. Vol. 3, 370), the benzylic alcohol (50 mmol) is dissolved in unhydrous dichloromethane (DCM) (about 100-150 mL) and the solution is cooled to about 00 (ice bath). To the solution is dropwise added a commercial 1.0 M solution of phosphorus tribromide (PBrGeneral procedure: General Procedure for the Bromination of Benzylic Alcohols to Benzylic Bromides [0571] Adapting literature known protocols (Harrison and Diehl, Org. Synth., 1955, Coll. Vol. 3, 370), the benzylic alcohol (50 mmol) is dissolved in anhydrous dichloromethane (DCM) (about 100-150 mL) and the solution is cooled to about 0° (ice bath). To the solution is dropwise added a commercial 1.0 M solution of phosphorus tribromide (PBrIF3a (0403) A mixture of IF2a (1.60 g, 9.58 mmol), CBr
Computed Properties
Molecular Weight:230.06
XLogP3:3.1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:228.97384
Monoisotopic Mass:228.97384
Topological Polar Surface Area:45.8
Heavy Atom Count:12
Complexity:169
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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2-BROMOMETHYL-1-METHYL-4-NITRO-BENZENE
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