3-BROMO-2-HYDROXY-5-METHYLPYRIDINE
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3-BROMO-2-HYDROXY-5-METHYLPYRIDINE
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CAS No:
17282-02-9
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Formula:
C6H6BrNO
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Chemical Name:
3-BROMO-2-HYDROXY-5-METHYLPYRIDINE
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Synonyms:
3-BROMO-5-METHYLPYRIDIN-2-OL;3-BROMO-5-METHYL-2(1H)-PYRIDINONE;3-BROMO-2-HYDROXY-5-METHYLPYRIDINE;TIMTEC-BB SBB003679;2-HYDROXY-3-BROMO-5-PICOLINE;3-Bromo-2-hydroxy-5-picoline;3-Bromo-2-hydroxy-5-methylpyridine 98%;3-Bromo-2-hydroxy-5-picoline 17282-02-9
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CAS No:
3-BROMO-2-HYDROXY-5-METHYLPYRIDINE Basic Attributes
188.02
186.963272
1423374
-0
DTXSID00395569
29333990
Characteristics
29.1
1
1.622±0.06 g/cm3(Predicted)
78-82 °C(lit.)
324.0±42.0 °C(Predicted)
131.1±25.9 °C
1.598
Keep Cold
0.000253mmHg at 25°C
Safety Information
III
1993
3
22-37/38-41-36/37/38
26-36/37/39-36
Xn,Xi
Irritant/Keep Cold
P261-P280-P305 + P351 + P338
H302-H315-H318-H335
|Danger|H302 (86.96%): Harmful if swallowed [Warning Acute toxicity, oral]|P261, P264, P270, P271, P280, P301+P312, P302+P352, P304+P340, P305+P351+P338, P310, P312, P321, P330, P332+P313, P337+P313, P362, P403+P233, P405, and P501|Aggregated GHS information provided by 46 companies from 6 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.
3-BROMO-2-HYDROXY-5-METHYLPYRIDINE Use and Manufacturing
5-Methyl-pyridin-2-ol (1 g, 9.16 mmol) was dissolved in 4 mL of CS2. Br2 (0.47 mL) was added thereto, andthe mixture was stirred at room temperature for 2 hours. Sodium thiosulfate (Na2S2O3) aqueous solution was addedthereto, and the reaction solution was extracted with EtOAc. The separated organic layer was dried with MgSO4 andconcentrated under reduced pressure to obtain the title compound (1.7 g, 98percent) in a solid form.1H-NMR (CDCl3) δ 7.73 (1H, s), 7.22 (1H, s), 2.10 (3H, s).3-Bromo-2-(difluoromethoxy)-5-methylpyridine 3-Bromo-2-(difluoromethoxy)-5-methylpyridine. To a solution of
Computed Properties
Molecular Weight:188.02
XLogP3:1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Exact Mass:186.96328
Monoisotopic Mass:186.96328
Topological Polar Surface Area:29.1
Heavy Atom Count:9
Complexity:205
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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3-BROMO-2-HYDROXY-5-METHYLPYRIDINE
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