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(+)-3-Bromocamphor

(+)-3-Bromocamphor structure

CAS No:
10293-06-8
Formula:
C10H15BrO
Chemical Name:
(+)-3-Bromocamphor
Synonyms:
Bicyclo[2.2.1]heptan-2-one,3-bromo-1,7,7-trimethyl-,(1R,3S,4S)-;2-Bornanone,3-bromo-,(1R,3S,4S)-(+)-;Bicyclo[2.2.1]heptan-2-one,3-bromo-1,7,7-trimethyl-,(1R-endo)-;Camphor,3α-bromo-,(+)-;(1R,3S,4S)-3-Bromo-1,7,7-trimethylbicyclo[2.2.1]heptan-2-one;endo-(+)-3-Bromo-2-bornanone;(+)-3-Bromocamphor;(+)-endo-3-Bromocamphor;(1R-endo)-(+)-3-Bromocamphor;(1R)-endo-3-Bromocamphor;(1R-endo)-3-Bromo-1,7,7-trimethylbicyclo[2.2.1]heptan-2-one
Categories:
Organic Chemistry > Phosphines

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(+)-3-Bromocamphor Basic Attributes

Molecular Weight：

231.13

Exact Mass：

231.13

EC Number：

233-652-1

HScode：

2914700090

Characteristics

PSA：

17.07000

XLogP3：

2.42

Appearance：

White Crystalline

Density：

1.4±0.1 g/cm3

Melting Point：

76 °C

Boiling Point：

274 °C

Flash Point：

35.8±9.9 °C

Refractive Index：

1.529

Storage Conditions：

2-8°C

Vapor Pressure：

0.028mmHg at 25°C

Specific rotation：

130 º (c=5, CH3OH)

Safety Information

Transport codes：

NONH for all modes of transport

wgk germany：

hazard class code：

36/37/38

safety instructions：

26-36-37/39

RTECS Number：

ED6750000

Marks：

Stability/Shelf Life：

Stable under normal temperatures and pressures.

Precautionary statement(s)：

P261-P305 + P351 + P338

Hazard Statements：

H315-H319-H335

(+)-3-Bromocamphor Use and Manufacturing

Methods of Manufacturing

Put camphor and a small amount of chloroform into the reaction pot, slowly add bromine below 90°C. After the addition, the temperature is increased to 115°C and kept at 115-130°C for nearly 3h. cool down. Crush to obtain α-bromocamphor.

Uses

Used as organic synthesis intermediate, pharmaceutical intermediate, and chiral structural unit

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