4-Bromo-5-methoxyquinoline
-
4-Bromo-5-methoxyquinoline
structure -
-
CAS No:
643069-46-9
-
Formula:
C10H8BrNO
-
Chemical Name:
4-Bromo-5-methoxyquinoline
-
Synonyms:
Quinoline,4-bromo-5-methoxy-;4-Bromo-5-methoxyquinoline
-
CAS No:
4-Bromo-5-methoxyquinoline Use and Manufacturing
A solution [OF QUINOLONE (C)] (3.2g, 18 mmol) in DMF (22 ml) was treated with phosphorous tribromide (2.2 ml). After 2 hours the mixture was added to water and neutralised with saturated aqueous sodium bicarbonate solution. Filtration and drying afforded a yellow solid (3.6g, 85percent). MS (+ve ion electrospray) m/z 239 [(MH+)]General procedure: To a stirred solution of the appropriate azine N-oxides in anhydrous CH