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4-BROMO-2-METHOXYBENZYL ALCOHOL97

4-BROMO-2-METHOXYBENZYL ALCOHOL97 structure

CAS No:
17102-63-5
Formula:
C8H9BrO2
Chemical Name:
4-BROMO-2-METHOXYBENZYL ALCOHOL97
Synonyms:
4-BROMO-2-METHOXYBENZYL ALCOHOL97;(4-broMo-2-Methoxyphenyl)Methanol;4-Bromo-2-methoxybenzyl alcohol 97%;(4-Bromo-2-methoxyphenyl);4-Bromo-2-methoxybenzyl alcohol≥ 99% (GC)
Categories:
Organic Chemistry > Hydrocarbons and Derivatives

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4-BROMO-2-METHOXYBENZYL ALCOHOL97 Basic Attributes

Molecular Weight：

217.061

Exact Mass：

215.97900

DSSTox ID：

DTXSID00568655

HScode：

2909499000

Characteristics

PSA：

29.5

XLogP3：

1.7

Density：

1.513g/cm3

Melting Point：

66-70 °C(lit.)

Boiling Point：

291℃

Flash Point：

130℃

Refractive Index：

1.57

Water Solubility：

Insoluble in water.

Safety Information

Transport codes：

NONH for all modes of transport

wgk germany：

hazard class code：

safety instructions：

24/25

Marks：

Precautionary statement(s)：

P264, P270, P301+P312, P330, P501

Hazard Statements：

H302

GHS Classification：

|Warning|H302 (88.64%): Harmful if swallowed [Warning Acute toxicity, oral]|P261, P264, P270, P271, P280, P301+P312, P302+P352, P304+P340, P305+P351+P338, P312, P321, P330, P332+P313, P337+P313, P362, P403+P233, P405, and P501|Aggregated GHS information provided by 44 companies from 3 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.

4-BROMO-2-METHOXYBENZYL ALCOHOL97 Use and Manufacturing

To a solution of methyl 4-bromo-2-methoxybenzoate (7.14g, 29mmol) in THF (35mL) was added a 2M solution of LiBHA mixture of General procedure: In general a mixture of various alcohols, dimethoxymethane (1:10 mole ratio) and 0.05 g of 10 Mo/ZrO2 was added and the mixture was refluxed at 40 °C for an appropriate time under nitrogen. The progress of the reaction was monitored by TLC. After completion of the reaction the mixture was cooled to room temperature filtered and the solid catalyst was washed with diethyl ether (5 mL). The filtrate was washed with brine solution and dried over anhydrous sodium sulphate. The solvent was evaporated in rota-vapour to get the residue. Thus obtained crude product was purified in silica gel (60-120) column chromatography by using suitable mobile phase pet ether-ethyl acetate (80:20) mixture. The isolated products are characterized by 1H and 13CNMR, GCMS spectroscopic.

Computed Properties

Molecular Weight:217.06
XLogP3:1.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:215.97859
Monoisotopic Mass:215.97859
Topological Polar Surface Area:29.5
Heavy Atom Count:11
Complexity:119
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

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(4-Bromo-2-methoxyphenyl)methanol

CAS No.: 17102-63-5

Content: 99.00%

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CAS No.: 17102-63-5

Grade: Industrial Grade

Content: 99%

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Guide of 4-BROMO-2-METHOXYBENZYL ALCOHOL97

Basic Attributes
Characteristics
Safety Information
Use and Manufacturing
Computed Properties
Recommended Suppliers
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4-BROMO-2-METHOXYBENZYL ALCOHOL97

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