Succinic acid menthol monoester
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Succinic acid menthol monoester
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CAS No:
77341-67-4
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Formula:
C14H24O4
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Chemical Name:
Succinic acid menthol monoester
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Synonyms:
Butanedioic acid,1-[(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl] ester;Butanedioic acid,mono[5-methyl-2-(1-methylethyl)cyclohexyl] ester,[1R-(1α,2β,5α)]-;Butanedioic acid,mono[(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl] ester;1-[(1R,2S,5R)-5-Methyl-2-(1-methylethyl)cyclohexyl] butanedioate;Physcool;Succinic acid menthol monoester;Physcool N 2188;FEMA 3810;754938-59-5
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CAS No:
Characteristics
63.6
3
white crystalline solid
1.1±0.1 g/cm3
60-62 °C
259.2°C at 760 mmHg
132.3±16.7 °C
1.478
insoluble in water
Succinic acid menthol monoester Use and Manufacturing
Synthetic Example 1(-)- Monomenthyl succinate was synthesized using the common method esterification of (-)-methanol and succinic anhydridein THF with the catalyst DMAP. Yield: 78.6percent. M.p. 61–63 °C.FR-IR (KBr, cm−1): 2917–3440, 1727, 1710, 1388, 1285, 1224, 1177, 1037, 1011. A dry Schlenk tube was charged with rac-alcohol (1 equivalent) and succinic anhydride (1 equiv.) dissolved in 2 mL of diethyl ether. The reaction was initiated by the addition of 100 mg of CCL. The reaction mixture was shaken at room temperature for 24 h. After removal of the lipase by filtration, the filtrate was shaken with 1 M Na
Food additives
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