1-BROMO-4-CHLORO-2-IODOBENZENE
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1-BROMO-4-CHLORO-2-IODOBENZENE
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CAS No:
148836-41-3
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Formula:
C6H3BrClI
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Chemical Name:
1-BROMO-4-CHLORO-2-IODOBENZENE
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Synonyms:
1-Bromo-4-chloro-2-iodobenzene;2-Bromo-5-chloroiodobenzene;Benzene, 1-bromo-4-chloro-2-iodo-;ACMC-209d19;SCHEMBL1627226;CTK4C5935;KS-00000DCL;DTXSID50679548;ZINC2567821;Benzene,1-bromo-4-chloro-2-iodo-
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CAS No:
1-BROMO-4-CHLORO-2-IODOBENZENE Use and Manufacturing
HCl (500ml) for 2-bromo-5-chloroaniline (50 g, 242.16 mmol) and the mixture stirred at 0 while NaNO2 (17.5g, 253.62 mmol) to H2O (50ml) was added dropwise dissolved in a -10 after 1 hour It was stirred. The KI (44.2g, 266.26mmol) was stirred was dropwise added, dissolved in H2O (50ml) one hour at 0 . After completion of the reaction with ethyl acetate and filter the solidExtracts were dried over MgSO4 and the organic layer was filtered under reduced pressure. The filtered organic layer was evaporated under reduced pressure to a rear purified by column chromatography to the desired compound 1-bromo-4-chloro-2-iodobenzene (62 g, Yield: 66percent) was obtained.
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