6-bromo-1-methyl-1H-indazol-3-amine

Intermediate 3. 6-bromo-1 -methyl-1 H-indazol-3-amine A solution of 6-bromo-1 /-/-indazol-3-amine (788mg, 3.71 mmol) in dimethylformamide (3ml_) was cooled to 0°C and sodium hydride (60percent of an oil dispersion; 163mg, 6.79mmol) was added in portions. The mixture was stirred for 30 minutes at 0°C. Methyl iodide (225μΙ_, 4.09mmol) was added into the mixture and stirred for 2 hours at room temperature. Water was added into the crude mixture and a red solid precipitates. The crude mixture was filtered and dried. A red solid was obtained as the title compound (80percent of yield). LRMS (m/z): 226 (M)

Molecular Weight:226.07
XLogP3:1.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Exact Mass:224.99016
Monoisotopic Mass:224.99016
Topological Polar Surface Area:43.8
Heavy Atom Count:12
Complexity:176
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes