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2-Bromo-1,10-phenanthroline

2-Bromo-1,10-phenanthroline structure

CAS No:
22426-14-8
Formula:
C12H7BrN2
Chemical Name:
2-Bromo-1,10-phenanthroline
Synonyms:
1,10-Phenanthroline,2-bromo-;2-Bromo-1,10-phenanthroline;2-Bromophenanthroline
Categories:
Pharmaceutical Intermediates > Bulk Drug Intermediates

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2-Bromo-1,10-phenanthroline Basic Attributes

Molecular Weight：

259.1

Exact Mass：

259.10

EC Number：

607-070-7

HScode：

2933990090

Characteristics

PSA：

25.8

XLogP3：

2.8

Density：

1.6±0.1 g/cm3

Melting Point：

161.0 to 165.0 °C

Flash Point：

204.3±23.2 °C

Refractive Index：

1.758

Safety Information

Transport codes：

UN2811 - class 6.1 - PG 3 - EHS - Toxic solids, organic, n.o.s., HI: all

hazard class code：

safety instructions：

26-39

Precautionary statement(s)：

P273-P280-P301 + P310 + P330-P305 + P351 + P338 + P310-P391-P501

Hazard Statements：

H301-H315-H318-H410

GHS Classification：

|Danger|H301 (100%): Toxic if swallowed [Danger Acute toxicity, oral]|P261, P264, P270, P271, P273, P280, P301+P310, P302+P352, P304+P340, P305+P351+P338, P310, P311, P312, P321, P322, P330, P332+P313, P337+P313, P361, P362, P363, P391, P403+P233, P405, and P501|Aggregated GHS information provided by 3 companies from 3 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.

2-Bromo-1,10-phenanthroline Use and Manufacturing

Reference Example 72-Bromo-1, 10-phenanthroline (7) [0129] [Chem. 24] [0130] Under a stream of argon, to compound (2) (10 g; 47.6 mmol), phosphorus pentabromide (28 g; 65 mmol) and phosphorus oxybromide (50 g; 174 mmol) were added at room temperature. The reaction temperature was raised to 80Production Example 72-Bromo-1, 10-phenanthroline (7)[0165] [Chem. 30] [0166] Under a stream of argon, to compound (2) (10 g; 47.6 mmol), phosphorus pentabromide (28 g; 65 mmol) and phosphorus oxybromide (50 g; 174 mmol) were added at room temperature. The reaction temperature was raised to 80General procedure: The procedure is identical to general procedure I, except that reactions were conducted at 0.2 M concentration with N-oxide (1.00 equiv), POBr1.2.

Computed Properties

Molecular Weight:259.10
XLogP3:2.8
Hydrogen Bond Acceptor Count:2
Exact Mass:257.97926
Monoisotopic Mass:257.97926
Topological Polar Surface Area:25.8
Heavy Atom Count:15
Complexity:234
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

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2-Bromo-1,10-phenanthroline

CAS No.: 22426-14-8

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Guide of 2-Bromo-1,10-phenanthroline

Basic Attributes
Characteristics
Safety Information
Use and Manufacturing
Computed Properties
Recommended Suppliers
Latest News
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2-Bromo-1,10-phenanthroline

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