4-Chloro-2-Methoxynicotinaldehyde
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4-Chloro-2-Methoxynicotinaldehyde
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CAS No:
1008451-58-8
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Formula:
C7H6ClNO2
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Chemical Name:
4-Chloro-2-Methoxynicotinaldehyde
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Synonyms:
4-Chloro-2-methoxynicotinaldehyde;4-chloro-2-methoxypyridine-3-carbaldehyde;4-CHLORO-2-METHOXY-PYRIDINE-3-CARBALDEHYDE;3-PYRIDINECARBOXALDEHYDE, 4-CHLORO-2-METHOXY-;SCHEMBL438652;DTXSID90696118;MFCD13188720;ZINC40449738;AB67001;AK-31452
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CAS No:
4-Chloro-2-Methoxynicotinaldehyde Use and Manufacturing
To a solution of LDA (1.0 M solution in hexane) (29.3 mL, 29.3 mmol) in THF (45 mL) was added a solution of 4-chloro-2-methoxypyridine (3.5 g, 24.38 mmol) in THF (8 mL) dropwise at -78 °C. The reaction mixture turned into light yellow solution and was stirred at-78 °C for 1 h, then DMF (3.78 mL, 48.8 mmol) was added dropwise. The reaction mixture was stirred at -78 °C for lh. The reaction mixture was quenched with saturated NH
4-Chloro-2-Methoxynicotinaldehyde
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