6-Chloro-2,5-dimethyl-4-pyrimidinamine
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6-Chloro-2,5-dimethyl-4-pyrimidinamine
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CAS No:
18260-92-9
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Formula:
C6H8ClN3
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Chemical Name:
6-Chloro-2,5-dimethyl-4-pyrimidinamine
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Synonyms:
6-chloro-2,5-dimethylpyrimidin-4-amine;BRN 0126825;Pyrimidine, 4-amino-6-chloro-2,5-dimethyl-;4-Amino-6-chloro-2,5-dimethylpyrimidine;4-Pyrimidinamine, 6-chloro-2,5-dimethyl-;6-chloro-2,5-dimethyl-pyrimidin-4-ylamine;5-25-10-00224 (Beilstein Handbook Reference);SCHEMBL259072;CTK8H3444;KS-00000RBP
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CAS No:
Characteristics
51.8
1.6
1.284±0.06 g/cm3(Predicted)
199.5-200.5 °C
279.7±35.0 °C(Predicted)
123ºC
1.586
6-Chloro-2,5-dimethyl-4-pyrimidinamine Use and Manufacturing
(c) 6-Chloro-2, 5-dimethylpyrirnidin-4-amine[00435] A microwave vial was charged with 4, 6-dichloro-2, 5-dimethylpyrimidine (523 mg, 2.95 mmol) and ammonium hydroxide (8 mL) in ethanol (4 mL). The vial was heated to 80 °C and stirred for 8 h. After concentration under reduced pressure, the reaction mixture was extracted with EtOAc (15 mL x 8). The combined organic layers were washed with brine (30 mL), dried over Na2S04 and concentrated to give 6-chloro-2, 5-dimethylpyrirnidin-4-amine as a yellow solid (411 mg). MS (ESI): m/z 158 [M+H]+.
6-Chloro-2,5-dimethyl-4-pyrimidinamine
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