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4-Picolyl chloride hydrochloride

4-Picolyl chloride hydrochloride structure

CAS No:
1822-51-1
Formula:
C6H6ClN.ClH
Chemical Name:
4-Picolyl chloride hydrochloride
Synonyms:
Pyridine,4-(chloromethyl)-,hydrochloride (1:1);Pyridine,4-(chloromethyl)-,hydrochloride;4-Picolyl chloride hydrochloride;4-(Chloromethyl)pyridine hydrochloride;4-(Chloromethyl)pyridinium chloride;4-Pyridylmethyl chloride hydrochloride;4-Chloromethylpyridine hydrochloride salt
Categories:
Pharmaceutical Intermediates > Bulk Drug Intermediates

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Description

YELLOW TO ORANGE FINE CRYSTALLINE POWDER

4-Picolyl chloride hydrochloride Basic Attributes

Molecular Weight：

164.03

Exact Mass：

162.995560

BRN：

3689154

EC Number：

217-350-7

NSC Number：

66483

DSSTox ID：

DTXSID00171264

HScode：

29333999

Characteristics

PSA：

12.9

Appearance：

Yellow to orange Fine Crystalline Powder

Melting Point：

165-166 °C

Flash Point：

102ºC

Refractive Index：

1.53

Water Solubility：

750 g/L (20 ºC)

Storage Conditions：

2-8°C

Safety Information

Packing level：

III

Hazard category：

Transport codes：

UN 3261 8/PG 3

wgk germany：

hazard class code：

34-4-22-36/37/38

safety instructions：

26-36/37/39-45-36

Marks：

C,Xi

Hazard note：

Corrosive

Precautionary statement(s)：

P280-P305 + P351 + P338-P310

Hazard Statements：

H314

GHS Classification：

|Danger|H302 (16.67%): Harmful if swallowed [Warning Acute toxicity, oral]|P260, P264, P270, P280, P301+P312, P301+P330+P331, P303+P361+P353, P304+P340, P305+P351+P338, P310, P321, P330, P363, P405, and P501|Aggregated GHS information provided by 48 companies from 6 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.

4-Picolyl chloride hydrochloride Use and Manufacturing

4-Chloromethylpyridine Hydrochloride (21); EMI35.0[0161] 4-Hydroxymethylpyridine (20) (54.4 g, 0.50 mol) was dissolved in acetonitrile 202 ml. The solution was added dropwise to a mixture of thionyl chloride (65.3 g, 0.55 mol) and acetonitrile (109 ml) under 50[deg.] C. The mixture was stirred at the same temperature for 1 hour, then cooled to room temperature to yield a slurry (quantitative) of the objective (21). [0162] <1>H-NMR (DMSO-TMS) [delta] ppm: 5.09 (s, 2H), 8.09 (d, J=6.6 Hz, 2H), 8.94 (d, J=6.6 Hz, 2H).(i)

Computed Properties

Molecular Weight:164.03
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:162.9955546
Monoisotopic Mass:162.9955546
Topological Polar Surface Area:12.9
Heavy Atom Count:9
Complexity:59.5
Covalently-Bonded Unit Count:2
Compound Is Canonicalized:Yes

Recommended Suppliers of 4-Picolyl chloride hydrochloride

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4-(Chloromethyl)pyridine hydrochloride

CAS No.: 1822-51-1

Content: 99.00%

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NANTONG REFORM PETRO-CHEMICAL CO.,LTD Contact Supplier

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4-(Chloromethyl)pyridine hydrochloride

CAS No.: 1822-51-1

Grade: Industrial Grade

Content: 99%

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Guide of 4-Picolyl chloride hydrochloride

Description
Basic Attributes
Characteristics
Safety Information
Use and Manufacturing
Computed Properties
Recommended Suppliers
Latest News
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4-Picolyl chloride hydrochloride

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