 Home > Encyclopedia > XPhos Pd G3

XPhos Pd G3

XPhos Pd G3 structure

CAS No:
1445085-55-1
Formula:
C46H62NO3PPdS
Chemical Name:
XPhos Pd G3
Synonyms:
XPhos-G3-Palladacycle
Categories:
Catalyst and Auxiliary > Precious Metal Catalysts

Request for Quotation

XPhos Pd G3 Basic Attributes

Molecular Weight：

847.45600

Exact Mass：

843.30700

Characteristics

PSA：

85.21000

XLogP3：

13.89620

Melting Point：

146-151°C (decomposition)

Safety Information

Transport codes：

NONH for all modes of transport

wgk germany：

safety instructions：

XPhos Pd G3 Use and Manufacturing

A 300-mL round-bottomed flask equipped with a stir bar and rubber septum was charged with μ-OMs dimer 3 (11.92 g, 15.25 mmol, 0.50 eq) and XPhos (14.52 g, 30.5 mmol, 1.00 eq). The flask was evacuated under vacuum and backfilled with argon (this procedure was repeated twice), after which THF (120 mL) was added. The reaction mixture was stirred at room temperature for 45 min. After removal of 90percent of the solvent under vacuum the product was precipitated from pentane to afford the title compound as an off-white solid as the 1:1 THF complex. THF could be removed by dissolving the solid in DCM and reprecipitating with pentane. Yield: 25.5 g, 92percent. FIG. 7. [0295] FIG. 8 tabulates the percent yield of various precatalysts formed using the procedures outlined above.A 300-mL round-bottomed flask equipped with a stir bar and rubber septum was charged with mu-OMs dimer 3 (11.92 g, 15.25 mmol, 0.50 eq) and XPhos (14.52 g, 30.5 mmol, 1.00 eq). The flask was evacuated under vacuum and backfilled with argon (this procedure was repeated twice), after which THF (120 mL) was added. The reaction mixture was stirred at room temperature for 45 min. After removal of 90% of the solvent under vacuum the product was precipitated from pentane to afford the title compound as an off-white solid as the 1:1 THF complex. THF could be removed by dissolving the solid in DCM and reprecipitating with pentane. Yield: 25.5 g, 92%. FIG. 7. [0295] FIG. 8 tabulates the % yield of various precatalysts formed using the procedures outlined above.

Recommended Suppliers of XPhos Pd G3

HANGZHOU LEAP CHEM CO., LTD. Contact Supplier

CN
5 YRS

Business licensed

Trader Supplier of Intermediates,Building blocks,API,Silicones,Peptides,Lab chemicals,Biochemicals,Pharmaceuticals,Screening Compounds,Food Additives

Methanesulfonato(2-dicyclohexylphosphino-2,4,6-tri-i-propyl-1,1-biphenyl)(2-aMino-1,1-biphenyl-2-yl)palladiuM(II), Min. 98% [XPhos Palladacycle]

CAS No.: 1445085-55-1

Content: 99.00%

Inquiry
Henan Lihao Chem Plant Limited Contact Supplier

CN
5 YRS

Business licensed

Trader Supplier of PVC resin,pvc paste resin,melamine

high quality XPhos Palladacycle Gen. 3 99% transparent liquid KANBEI

CAS No.: 1445085-55-1

Grade: Industrial Grade

Content: 99%

Inquiry
Henan Ouber Technology Co., Ltd. Contact Supplier

CN
7 YRS

Business licensed Certified factory

Manufactory Supplier of OLED intermedaites,Pharmaceutical intermediates,Ligands and catalysts

XPhos Pd G3 / 1445085-55-1

CAS No.: 1445085-55-1

Grade: Chemical Grade

Content: 99%

Inquiry
Honour Enterprise Company Limited Contact Supplier

CN
4 YRS

Business licensed

Trader Supplier of Semaglutide,Tirzepatide,API,Enzyme

More than 15 years GMP Factory Suppy 99.5% (SP-4-3)-[2'-(Amino)[1,1'-biphenyl]-2-yl][dicyclohexyl[2',4',6'-tris(1-methylethyl)[1,1'- Medical Grade CAS

CAS No.: 1445085-55-1

Grade: Pharmaceutical Grade

Content: 99.5%

Inquiry