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2,3,4,6-Tetrakis-O-trimethylsilyl-D-gluconolactone

2,3,4,6-Tetrakis-O-trimethylsilyl-D-gluconolactone structure

CAS No:
32384-65-9
Formula:
C18H42O6Si4
Chemical Name:
2,3,4,6-Tetrakis-O-trimethylsilyl-D-gluconolactone
Synonyms:
D-Gluconic acid,2,3,4,6-tetrakis-O-(trimethylsilyl)-,δ-lactone;Gluconic acid,2,3,4,6-tetrakis-O-(trimethylsilyl)-,δ-lactone,D-;2,3,4,6-Tetrakis-O-trimethylsilyl-D-gluconolactone;(3R,4S,5R,6R)-3,4,5-Tris[(trimethylsilyl)oxy]-6-[[(trimethylsilyl)oxy]methyl]tetrahydropyran-2-one;(3R,4S,5R,6R)-3,4,5-Tri[(trimethylsilyl)oxy]-6-[[(trimethylsilyl)oxy]methyl]tetrahydro-2H-pyran-2-one;(3R,4S,5R,6R)-3,4,5-Tris(trimethylsilyloxy)-6-[(trimethylsilyloxy)methyl]tetrahydro-2H-pyran-2-one;2,3,4,6-Tetra-O-(trimethylsilyl)-D-glucono-1,5-lactone;55515-29-2
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Description

Pale yellow oil

2,3,4,6-Tetrakis-O-trimethylsilyl-D-gluconolactone Basic Attributes

Molecular Weight：

466.865

Exact Mass：

466.86

EC Number：

608-732-8

Characteristics

PSA：

63.22000

XLogP3：

4.42360

Density：

1.0±0.1 g/cm3

Boiling Point：

417.2±45.0 °C at 760 mmHg

Flash Point：

171.3±24.3 °C

Refractive Index：

1.445

Analysis Methods

Name	Column Shape	Active Phase(℃)	Retention index	Method	Comments	Reference
Van Den Dool and Kratz RI, non-polar column, temperature ramp	Capillary	VF-5MS	1878.	temperature ramp	30. m/0.25 mm/0.25 μm, He; T_start: 60. C; T_end: 270. C	Tretyakov, K.V.Retention Data (March 2011). NIST Mass Spectrometry Data Center.NIST Mass Spectrometry Data Center, 2011.
Van Den Dool and Kratz RI, non-polar column, temperature ramp	Capillary	Polydimethyl siloxane with 5 % phenyl groups	1873.	custom temperature program	Program: not specified	Kempa, S.Hummel, J.Schwemmer, T.Pietzke, M.Strehmel, N.Wienkoop, S.Kopka, J.Weckwerth, W.An automated GCxGC-TOF-MS protocol for batch-wise extraction and alinmebt of mass isotopomer matrixes from differential 13C-labeling experiments: a case study for photoautotrophic-mixotrophic grown Chlamydomonas reinhardtii cellsJ. Basic Microbiol.2009, 49, 1, 82-91.
Van Den Dool and Kratz RI, non-polar column, temperature ramp	Capillary	VF-5MS	1874.7	custom temperature program	30. m/0.25 mm/0.25 μm, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C	Tret'yakov, K.V.Retention Data. NIST Mass Spectrometry Data Center.NIST Mass Spectrometry Data Center, 2007.

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Guide of 2,3,4,6-Tetrakis-O-trimethylsilyl-D-gluconolactone

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Basic Attributes
Characteristics
Analysis Methods
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