2,4-bis(trimethylsilyloxy)-6-aza-5-methylpyrimidine
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2,4-bis(trimethylsilyloxy)-6-aza-5-methylpyrimidine
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CAS No:
17331-64-5
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Formula:
C10H21N3O2Si2
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Chemical Name:
2,4-bis(trimethylsilyloxy)-6-aza-5-methylpyrimidine
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Synonyms:
6-Methyl-3,5-bis-trimethylsilyloxy-1,2,4-triazin;b;6-Methyl-3.5-bis(trimethylsiloxy)1,2,4-triazine;6-methyl-3,5-bis(trimethylsiloxy)-1,2,4-triazine;6-Methyl-3,5-bis-(trimethylsilyloxy)-1,2,4-triazin;6-methyl-3,5-bis-trimethylsilanyloxy-[1,2,4]triazine;
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CAS No:
Analysis Methods
| Name | Column Shape | Active Phase(℃) | Retention index | Temperature Control | Method | Comments | Reference |
|---|---|---|---|---|---|---|---|
| Kovats' RI, non-polar column, isothermal | Packed | OV-101 | 1459.8 | 160. | isothermal | Ar, AW-DMCS Chromosorb W HP; Column length: 2. m | Miller, V.Pacáková, V.Smolková, E.Gas-liquid chromatographic analysis of trimethylsilyl derivatives of pyrimidine and purine bases and nucleosidesJ. Chromatogr.1976, 119, 355-367. |
| Kovats' RI, non-polar column, isothermal | Packed | SE-30 | 1500. | 150. | isothermal | Pacakova, V.Miller, V.Cernohorsky, I.J.Gas-Liquid Chromatography of Some Pyrimidine DerivativesAnal. Biochemistry1971, 42, 2, 549-554. | |
| Kovats' RI, non-polar column, isothermal | Packed | OV-101 | 1500. | 150. | isothermal | Pacakova, V.Miller, V.Cernohorsky, I.J.Gas-Liquid Chromatography of Some Pyrimidine DerivativesAnal. Biochemistry1971, 42, 2, 549-554. | |
| Kovats' RI, non-polar column, isothermal | Capillary | VF-5MS | 1467.6 | custom temperature program | 30. m/0.25 mm/0.25 μm, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C | Tret'yakov, K.V.Retention Data. NIST Mass Spectrometry Data Center.NIST Mass Spectrometry Data Center, 2007. |
Guide of 2,4-bis(trimethylsilyloxy)-6-aza-5-methylpyrimidine
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