lanosterol TMS ether
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lanosterol TMS ether
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CAS No:
55493-84-0
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Formula:
C33H58OSi
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Chemical Name:
lanosterol TMS ether
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Synonyms:
[(3S,5R,10S,13R,14R,17R)-17-((R)-1,5-Dimethyl-hex-4-enyl)-4,4,10,13,14-pentamethyl-2,3,4,5,6,7,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yloxy]-trimethyl-silane;lanosterol-3-TMS;
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CAS No:
Analysis Methods
| Name | Column Shape | Active Phase(℃) | Retention index | Temperature Control | Method | Comments | Reference |
|---|---|---|---|---|---|---|---|
| Van Den Dool and Kratz RI, non-polar column, temperature ramp | Capillary | DB-5MS | 3335. | temperature ramp | 10. m/0.18 mm/0.18 μm, 70. C @ 2. min, 40. K/min, 320. C @ 2. min | Jonsson, P.Johansson, A.I.Gullberg, J.Trygg, J.Jiye, A.Grung, B.Marklund, S.Sjöström, M.Antti, H.Moritz, T.High-throughput data analysis for detecting and identifying differences between samples in GC/MS-based metabolomic analysesAnal. Chem.2005, 77, 17, 5635-5642. | |
| Van Den Dool and Kratz RI, non-polar column, temperature ramp | Capillary | OV-1 | 3327. | temperature ramp | 1. K/min; Column length: 25. m; Column diameter: 0.32 mm; Tstart: 220. C; Tend: 75. C | le Fur, Y.Maume, G.Feuillat, M.Maume, B.F.Characterization by gas chromatography/mass spectrometry of sterols in Saccharomyces cerevisiae during autolysisJ. Agric. Food Chem.1999, 47, 7, 2860-2864. | |
| Van Den Dool and Kratz RI, non-polar column, temperature ramp | Capillary | SE-30 | 3327. | temperature ramp | 30. m/0.32 mm/0.25 μm, He, 2. K/min; Tstart: 220. C | Le Fur, Y.Maume, G.Feuillat, M.Maume, B.F.Characterization by gas chromatography/mass spectrometry of sterols in Saccharomyces cerevisiae during autolysisJ. Agric. Food Chem.1999, 47, 7, 2860-2864. |
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