Trimethylsilyl-gluconsaeure
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Trimethylsilyl-gluconsaeure
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CAS No:
34290-52-3
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Formula:
C24H60O7Si6
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Chemical Name:
Trimethylsilyl-gluconsaeure
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Synonyms:
2-O,3-O,4-O,5-O,6-O-Pentakis(trimethylsilyl)-D-gluconic acid trimethylsilyl ester;34290-52-3
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CAS No:
Analysis Methods
| Name | Column Shape | Active Phase(℃) | Retention index | Temperature Control | Method | Comments | Reference |
|---|---|---|---|---|---|---|---|
| Kovats' RI, non-polar column, isothermal | Packed | OV-1 | 2068. | 160. | isothermal | N2, Chromosorb G (100-120 mesh); Column length: 2. m | Petersson, G.Retention Data in GLC Analysis; Carbohydrate-Related Hydroxy Carboxylic and Dicarboxylic Acids as Trimethylsilyl DerivativesJ. Chromatogr. Sci.1977, 15, 7, 245-255. |
| Kovats' RI, non-polar column, isothermal | Capillary | RTX-5Sil | 1997.0 | temperature ramp | 80. C @ 2. min, 18. K/min, 350. C @ 2. min; Column length: 30. m; Column diameter: 0.25 mm | Wagner, C.Sefkow, M.Kopka, J.Construction and application of a mass spectral and retention time index database generated from plant GC/EI-TOF-MS metabolite profilesPhytochemistry2003, 62, 6, 887-900. | |
| Kovats' RI, non-polar column, isothermal | Capillary | Ultra-2 | 2043. | temperature ramp | 25. m/0.31 mm/0.52 μm, He, 5. K/min; Tstart: 50. C; Tend: 300. C | Tuchman, M.Bowers, L.D.Fregien, K.D.Crippin, P.J.Krivit, W.Capillary Gas Chromatographic Separation of Urinary Organic Acids. Retention Indices of 101 Urinary Acids on a 5% Phenylmethyl Silicone Capillary ColumnJ. Chromatogr. Sci.1984, 22, 5, 198-202. | |
| Kovats' RI, non-polar column, isothermal | Capillary | HP-5MS | 2037. | temperature ramp | 30. m/0.25 mm/0.25 μm, He, 70. C @ 3. min, 4. K/min, 280. C @ 3. min | Lee, B.Y.Yanamandra, K.Thurmon, T.F.Quantitative estimation of organic analytes with a capillary columnAm. Clin. Lab.2002, May, 30-34. |
Guide of Trimethylsilyl-gluconsaeure
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