(3R,10S,13S)-3-((tert-butyldimethylsilyl)oxy)-10,13-dimethylhexadecahydro-17H-cyclopenta[a]phenanthren-17-one
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(3R,10S,13S)-3-((tert-butyldimethylsilyl)oxy)-10,13-dimethylhexadecahydro-17H-cyclopenta[a]phenanthren-17-one
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CAS No:
57711-45-2
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Formula:
C25H44O2Si
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Chemical Name:
(3R,10S,13S)-3-((tert-butyldimethylsilyl)oxy)-10,13-dimethylhexadecahydro-17H-cyclopenta[a]phenanthren-17-one
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Synonyms:
3-O-(tert-butyldimethylsilyl)androsterone;Androsteron-tert-butyldimethylsilylether;Androsterone-dimethyl-tert.-butylsilyl-ether;(3R,5S,8R,9S,10S,13S,14S)-3-(tert-Butyl-dimethyl-silanyloxy)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-one;(3α,5α)-3-{[tert-butyl(dimethyl)silyl]oxy}androstan-17-one;3α-t-Butyl-dimethylsilyloxy-5α-androstan-17-on;3α-(t-butyldimethylsiloxy)-5α-androstan-17-one;
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CAS No:
(3R,10S,13S)-3-((tert-butyldimethylsilyl)oxy)-10,13-dimethylhexadecahydro-17H-cyclopenta[a]phenanthren-17-one Basic Attributes
404.7
404.311
Analysis Methods
| Name | Column Shape | Active Phase(℃) | Retention index | Temperature Control | Method | Comments | Reference |
|---|---|---|---|---|---|---|---|
| Kovats' RI, non-polar column, isothermal | Packed | OV-1 | 2702. | 230. | isothermal | Gas Chrom Q; Column length: 1. m | Quilliam, M.A.Westmore, J.B.Sterically crowded trialkylsilyl derivatives for chromatography and mass spectrometry of biologically-important compoundsAnal. Chem.1978, 50, 1, 59-68. |
| Kovats' RI, non-polar column, isothermal | Packed | OV-1 | 2740. | 260. | isothermal | Gas Chrom Q; Column length: 1. m | Quilliam, M.A.Westmore, J.B.Sterically crowded trialkylsilyl derivatives for chromatography and mass spectrometry of biologically-important compoundsAnal. Chem.1978, 50, 1, 59-68. |
| Kovats' RI, non-polar column, isothermal | Capillary | VF-5MS | 2788.8 | custom temperature program | 30. m/0.25 mm/0.25 μm, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C | Tret'yakov, K.V.Retention Data. NIST Mass Spectrometry Data Center.NIST Mass Spectrometry Data Center, 2007. |
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