Methyl4-methyl-5-thiazolecarboxylate
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Methyl4-methyl-5-thiazolecarboxylate
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CAS No:
81569-44-0
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Formula:
C6H7NO2S
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Chemical Name:
Methyl4-methyl-5-thiazolecarboxylate
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Synonyms:
METHYL 4-METHYL-5-THIAZOLYL FORMATE;METHYL 4-METHYLTHIAZOLE-5-CARBOXYLATE;Methyl 4-methyl-5-thiazolecarboxylate;Methyl,1-4-methyl-5-thiazolecarboxylate;methyl 4-methyl-1,3-thiazole-5-carboxylate;4-METHYLTHIAZOLE-5-CARBOXYLIC ACID METHYL ESTER;5-Thiazolecarboxylicacid, 4-Methyl-, Methyl ester
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CAS No:
Methyl4-methyl-5-thiazolecarboxylate Use and Manufacturing
General procedure: A solution of amine 2 (5 mmol) in THF (3 mL) was added dropwise over 20 min to a solution of t-BuONO (7.5 mmol) and DMSO (0.5 mmol) in THF (7 mL) at 30 °C. The mixture was stirred at 30 °C until the starting materials 2 were consumed (monitored by TLC). The solvent was evaporated, and the yields of the low boiling point products were determined by GC; the high boiling point products were isolated by column chromatography on silica gel (hexane/ethyl acetate).Silver reagent (0.1 mmol), phosphine ligand (0.1 mmol), deuterated water (0.4 g, 20 mmol), General procedure: A solution of amine 2 (5 mmol) in THF (3 mL) was added dropwise over 20 min to a solution of t-BuONO (7.5 mmol) and DMSO (0.5 mmol) in THF (7 mL) at 30 C. The mixture was stirred at 30 C until the starting materials 2 were consumed (monitored by TLC). The solvent was evaporated, and the yields of the low boiling point products were determined by GC; the high boiling point products were isolated by column chromatography on silica gel (hexane/ethyl acetate).
Computed Properties
Molecular Weight:157.19
XLogP3:1.5
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:157.01974964
Monoisotopic Mass:157.01974964
Topological Polar Surface Area:67.4
Heavy Atom Count:10
Complexity:140
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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Methyl4-methyl-5-thiazolecarboxylate
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